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Resin-based activated carbon ball and preparation method thereof

An activated carbon ball, resin-based technology, applied in separation methods, chemical instruments and methods, other chemical processes, etc., can solve the problem that resin-based activated carbon is not suitable for adsorbing desulfurizers, etc., and achieve the effect of good fluidity

Inactive Publication Date: 2015-12-23
BLUESTAR CHENGDU NEW MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The present invention aims to solve the problem that the resin-based activated carbon in the prior art is not suitable for adsorbing desulfurizing agents, and provides a resin-based activated carbon ball, which has good performance and is very suitable for adsorbing desulfurizing agents

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] A resin-based activated carbon sphere, comprising the following raw materials in parts by weight:

[0033] 10 parts m-ethylphenol

[0034] Formaldehyde 20 parts

[0035] 5 parts of triethylamine

[0036] 80 parts of deionized water

[0037] 3 parts polyvinyl alcohol

[0038] 10 parts melamine

[0039] 10 parts of inorganic salt.

Embodiment 2

[0041] A resin-based activated carbon sphere, comprising the following raw materials in parts by weight:

[0042] 15 parts m-ethylphenol

[0043] Formaldehyde 55 parts

[0044] 9 parts of triethylamine

[0045] 120 parts of deionized water

[0046] 8 parts polyvinyl alcohol

[0047] 20 parts of melamine

[0048] 25 parts of inorganic salts.

Embodiment 3

[0050] A resin-based activated carbon sphere, comprising the following raw materials in parts by weight:

[0051] 13 parts m-ethylphenol

[0052] 38 parts of formaldehyde

[0053] 7 parts of triethylamine

[0054] 100 parts of deionized water

[0055] 5.5 parts of polyvinyl alcohol

[0056] 15 parts melamine

[0057] 18 parts of inorganic salts.

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PUM

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Abstract

The invention relates to a resin-based activated carbon ball and a preparation method thereof, belonging to the technical field of high polymer materials. The resin-based activated carbon ball is prepared from the following materials according to parts by weight: 10-15 parts of m-ethyl phenol, 20-55 parts of formaldehyde, 5-9 parts of triethylamine, 80-120 parts of deionized water, 3-8 parts of polyvinyl alcohol, 10-20 parts of melamine and 10-25 parts of inorganic salt. According to the invention, spherical phenolic resin is synthesized first so as to be used as basic resin for preparing resin-based activated carbon, and then, the resin-based activated carbon is prepared at high temperature under protection of nitrogen. Compared with powdery and granular activated carbon, the spherical activated carbon becomes an adsorptive desulfurizing agent with excellent performance depending on the characteristics of smooth surface, suitable ball diameter and good mobility.

Description

Technical field [0001] The present invention involves a activated carbon and its preparation methods. More specifically, the invention involves a resin -based activated carbon ball and its preparation method, which is a high molecular material technology field. technical background [0002] Activated carbon has the characteristics of cheap raw materials, higher surface area, large Kong Rong, and easy regeneration, which are widely used to adsorb desulfurization.At present, activated carbon research mainly includes the following aspects: First, the impact of hole structure on adsorption performance. The use of polystyrene activated carbon balls to adsorb DBT in the simulation oil. The DBT capacity is 109.36mg / g.There is a good correlation between the holes (0.7nm) of the holes (the aperture diameter <0.7nm), and there is no correlation between the comparison surface area of the activated carbon ball and the total Kong Rong.Second, the activated carbon surface loaded metal oxide...

Claims

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Application Information

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IPC IPC(8): B01J20/20B01J20/30B01D53/02
Inventor 曹先军王凤德赵奕崔晓静高川刘咏梅
Owner BLUESTAR CHENGDU NEW MATERIALS
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