Preparation method for nickel-based alloy ingot
A nickel-based alloy and nickel powder technology is applied in the field of preparation of nickel-based alloy ingots, which can solve the problems of difficulty in obtaining alloy ingots, unfavorable thermal-mechanical processing of alloy ingots, etc., and achieves the effects of ensuring composition uniformity and increasing costs.
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Embodiment 1
[0021] This embodiment includes the following steps:
[0022] Step 1, uniformly mix nickel powder and metal element powder to obtain a mixed powder, then press the mixed powder to obtain a pre-sintered block; the metal element powder is tungsten powder, and the mass content of the tungsten powder in the mixed powder is 14 %, the balance is nickel powder;
[0023] Step 2: Sintering the pre-sintered block under the protection of hydrogen to obtain a pre-sintered block; the temperature of the sintering process is 1200° C., and the time is 2 hours;
[0024] Step 3. Place the pre-melted block described in step 2 in a medium-frequency induction melting furnace, and perform medium-frequency induction melting treatment under the condition that the pressure in the furnace is less than 10 Pa to obtain a nickel-based alloy melt with a temperature of 1800° C., and then melt the The nickel-based alloy melt is cast under the condition that the degree of vacuum is not greater than 100Pa to ...
Embodiment 2
[0044] This embodiment includes the following steps:
[0045] Step 1, uniformly mix nickel powder and metal element powder to obtain a mixed powder, then press the mixed powder to obtain a pre-sintered block; the metal element powder is tungsten powder, and the mass content of the tungsten powder in the mixed powder is 1 %, the balance is nickel powder;
[0046] Step 2: Sintering the pre-sintered block under the protection of hydrogen to obtain a pre-sintered block; the temperature of the sintering process is 1000° C., and the time is 4 hours;
[0047]Step 3. Place the pre-melted block described in step 2 in an intermediate frequency induction melting furnace, and carry out intermediate frequency induction melting treatment under the condition that the pressure in the furnace is less than 10 Pa to obtain a nickel-based alloy melt with a temperature of 1600° C. The nickel-based alloy melt is cast under the condition that the degree of vacuum is not greater than 100Pa to obtain...
Embodiment 3
[0054] This embodiment includes the following steps:
[0055] Step 1, uniformly mix nickel powder and metal element powder to obtain a mixed powder, then press the mixed powder to obtain a pre-sintered block; the metal element powder is tungsten powder, and the mass content of the tungsten powder in the mixed powder is 24 %, the balance is nickel powder;
[0056] Step 2, sintering the pre-sintered block under the protection of hydrogen to obtain a pre-fritted block; the temperature of the sintering process is 1100° C., and the time is 3 hours;
[0057] Step 3. Place the pre-melted block described in step 2 in an intermediate frequency induction melting furnace, and perform intermediate frequency induction melting treatment under the condition that the pressure in the furnace is less than 10Pa to obtain a nickel-based alloy melt with a temperature of 1700°C, and then melt the The nickel-based alloy melt is cast under the condition that the degree of vacuum is not greater than ...
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