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Preparation method of wild chrysanthemum natural dye and preparation of anti-bacterial textiles adopting wild chrysanthemum natural dye

A natural dye, the technology of wild chrysanthemum, applied in the preparation and application of natural dyes, can solve the problems of unsuitable textile application and promotion, general antibacterial effect, poor extraction effect, etc., and achieve great use value, safe wearing, and short time effect

Active Publication Date: 2015-11-18
义乌市华越新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] After searching the prior art documents, it was found that Shen Haijin and others published in the "Journal of Plant Resources and Environment" published in "The composition of phenolic components of 60% ethanol extract of wild chrysanthemum and its ability to scavenge free radicals and prevent mildew" in the article Mainly carried out analysis and research on the extraction of wild chrysanthemum and the composition and content of phenolic components. The extractant is a certain concentration of ethanol solution, and no other extractant is added. This method not only has poor extraction effect, but also takes a long time to extract (2 ~24h); People such as Nateepat Pitinidhipat pointed out in the article "Antibacterial Activity of Chrysanthemumindicum, Centellaasiatica and Andrographis paniculata against Bacillus cereus and Listeriamonocytogenes under Osmotic Stress" published in "Technical Report" that the wild chrysanthemum extract has certain antibacterial properties to Bacillus, Listeria; Poor, and its antibacterial effect is general, not suitable for the application and promotion of textiles
[0005] At present, the research on wild chrysanthemum is limited to traditional Chinese medicine and food coloring, and there is no report about the preparation method of wild chrysanthemum natural dye antibacterial functional textiles

Method used

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  • Preparation method of wild chrysanthemum natural dye and preparation of anti-bacterial textiles adopting wild chrysanthemum natural dye

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Embodiment 1

[0031] Wash the wild chrysanthemum, dry it, and mechanically crush it, weigh 1 kg of the crushed wild chrysanthemum, add it to 10 kg of ethanol aqueous solution containing sodium carbonate, and extract at 90°C for 30 minutes to obtain the extract; take a small amount of extract, It was obtained after ultraviolet spectrum analysis in the accompanying drawing figure 1 The UV-Vis absorption spectrum. Wherein, the mass percent concentration of ethanol in the ethanol aqueous solution is 20%, and every kilogram of ethanol aqueous solution contains 0.5 g of sodium carbonate. Then, the extract was filtered and concentrated to 5 kg by distillation under reduced pressure to obtain concentrated wild chrysanthemum natural dye.

[0032] Depend on figure 1 It was found that the maximum absorption wavelength of the ground chrysanthemum was 300 to 350 nm.

Embodiment 2

[0034] Wash the wild chrysanthemum flower, dry it in the air, crush it mechanically, weigh 1 kg of the crushed wild chrysanthemum flower, add it to 20 kg of ethanol aqueous solution containing sodium carbonate, and extract it at 75°C for 70 minutes to obtain the extract. Wherein, the mass percent concentration of ethanol in the ethanol aqueous solution is 30%, and every kilogram of ethanol aqueous solution contains 1g of sodium carbonate. Then the extract was filtered and concentrated to 5 kg by distillation under reduced pressure to obtain the concentrated wild chrysanthemum natural dye.

Embodiment 3

[0036] Wash the wild chrysanthemum flower, dry it in the air, crush it mechanically, weigh 1 kg of the crushed wild chrysanthemum flower, add it to 30 kg of ethanol aqueous solution containing sodium carbonate, and extract at 60°C for 120 minutes to obtain the extract. Wherein, the mass percentage concentration of ethanol aqueous solution ethanol is 40%, contains sodium carbonate 1.5g in every kilogram of ethanol aqueous solution. Then the extract was filtered and concentrated to 5 kg by distillation under reduced pressure to obtain the concentrated wild chrysanthemum natural dye.

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Abstract

The invention discloses a preparation method of wild chrysanthemum natural dye and preparation of anti-bacterial textiles adopting the wild chrysanthemum natural dye. The preparation method of the wild chrysanthemum natural dye is as follows: smashed wild chrysanthemum is added to an ethanol water solution, is subjected to reflux extraction for 0.5-2 h at the temperature ranging from 60 DEG C to 90 DEG C, an extracting solution is obtained, and the concentrated wild chrysanthemum natural dye is obtained by treating the extracting solution; the ethanol water solution comprises, in percentage by mass, 10%-40% of ethanol, each kilogram of the ethanol water solution contains 0.5-1.5 g of sodium carbonate, the mass ratio of the smashed wild chrysanthemum to the ethanol water solution is 1:(10-30), and the mass of the concentrated wild chrysanthemum natural dye is 1 / 6-1 / 2 of that of the ethanol water solution . Environmental pollution cannot be caused in the extraction process of the wild chrysanthemum natural dye, the extracting solution is taken as a dyeing agent and used for dyeing protein fiber, then the protein fiber has good anti-bacterial performance, soft color and luster and good color fastness, and the textiles made of the protein fiber are safe and comfortable to wear.

Description

technical field [0001] The invention relates to the preparation and application of natural dyes, in particular to a preparation method of wild chrysanthemum natural dyes and the preparation of antibacterial textiles. Background technique [0002] Natural dyes are mainly extracted from plant rhizomes, fruit shells, etc., which have good compatibility with the ecological environment and can be biodegraded. Some natural plant dyes come from Chinese herbal medicines. Besides dyeing, they also have the function of medicine and health care. Therefore, natural dyes have broad application prospects in the fields of high-grade real silk products, home textile products and decorations. [0003] Wild chrysanthemum is a perennial herb of Compositae. Mainly distributed in Jilin, Liaoning, Hebei, Henan and other places in China. Existing data show that wild chrysanthemum contains a variety of pharmacologically active ingredients, including luteolin, chrysanthemum ketone (birrhanonediol...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09B61/00D06P3/04D06P3/14D06P1/34D06P1/673
CPCC09B61/00D06P1/34D06P1/6735D06P3/04D06P3/14
Inventor 余志成刘文凤
Owner 义乌市华越新材料科技有限公司
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