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A kind of detection method of sare thirteen flavor penniao preparation

A detection method, the technology of thirteen flavors, applied in the field of medicine, can solve the problems of small prescription volume, many medicinal flavors, unclear active ingredients, etc., and achieve the effect of product quality and safety

Active Publication Date: 2016-09-07
JINKE TIBETAN MEDICINE QINGHAI PROV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0025] To sum up, since most of the prescriptions of Tibetan medicines have many flavors and small amounts of prescriptions, the active ingredients are not clear, and animal medicines and mineral medicines are commonly used, the key medicinal materials of the prescriptions cannot be fully followed in accordance with the principle of monarch, minister, assistant, and envoy in traditional Chinese medicine. Quality Control

Method used

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  • A kind of detection method of sare thirteen flavor penniao preparation
  • A kind of detection method of sare thirteen flavor penniao preparation
  • A kind of detection method of sare thirteen flavor penniao preparation

Examples

Experimental program
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Effect test

experiment example 1

[0070] Experimental example 1: identification method

[0071] Sare Thirteen Flavored Pengniao Pills are provided by Qinghai Jinhe Tibetan Medicine Pharmaceutical Co., Ltd.

[0072] A. Myrobalan

[0073] Take 5g of Sare Thirteen Wei Pengniao Wan fine powder, add 25ml of methanol, ultrasonically extract for 1 hour, filter, and use it as the test solution. Take an appropriate amount of gallic acid reference substance, add methanol to make a solution containing 1mg per 1ml, as the reference substance solution. Take 2 μl of each of the above two solutions, spot on the same silica gel G thin-layer plate, develop with tetrahydrofuran-isopropanol-glacial acetic acid as the developer, take it out, dry it in the air, and spray it with 2% ferric chloride at a weight-volume ratio Ethanol solution, heated at 105°C until the spots are clearly colored.

[0074] Result analysis: Tetrahydrofuran-isopropyl (4:3:0.5), (6:4:1), (8:5:2) with a volume ratio of 4-8:3-5:0.5-2 Under the condition ...

experiment example 2

[0081] Experimental example 2: Aconitine limit inspection

[0082] Take 15g of Sare Shisanwei Pengniaowan fine powder, weigh it accurately, add 100ml of diethyl ether, add 20ml of ammonia test solution, ultrasonicate for 30 minutes, let stand overnight, filter, transfer the filtrate to a separatory funnel, add 5% hydrochloric acid Shake 40ml of the solution, stand still, separate layers, separate the acid solution, add 30ml of 5% hydrochloric acid solution to the ether layer, shake, stand still, separate layers, separate the acid solution and combine with the above acid solution, add ammonia to test solution to adjust the pH value to 9-10, then shake and extract with diethyl ether 3 times, 20ml each time, evaporate the ether solution to dryness, dissolve the residue with absolute ethanol and dilute to 2ml, and use it as the test solution. Take another aconitine reference substance, add absolute ethanol to make a solution containing 0.2mg per 1ml, as the reference substance sol...

Embodiment 1

[0098] A detection method for a sare thirteen-flavored penniao preparation, comprising:

[0099] A. Identification of Myrobalan

[0100] Take 5g of Sare thirteen flavor Pengniao preparation powder, add 25ml of methanol, ultrasonically extract for 1 hour, filter, and use it as the test solution. Take an appropriate amount of gallic acid reference substance, add methanol to make a solution containing 1mg per 1ml, as the reference substance solution. Take 2 μl of each of the above two solutions, spot on the same silica gel G thin-layer plate, and use tetrahydrofuran-isopropanol-glacial acetic acid as the developer with a volume-to-part ratio of 6:4:1, develop, take out, dry in the air, and spray Use 2% ferric chloride ethanol solution at a weight-to-volume ratio and heat at 105°C until the spots are clearly colored. In the chromatogram of the test product, there are spots of the same or similar color at the position corresponding to the chromatogram of the reference product.

...

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Abstract

The present invention relates to a detection method for a sare thirteen-flavored penniao preparation provided by the present invention. On the basis of the original standard, the present invention adds the identification of chebula, woody, nutmeg and musk of precious medicinal materials, and adds the inspection of aconitine in the iron club, which further ensures the safety, uniformity, effectiveness and controllable quality of the product.

Description

technical field [0001] The invention relates to a detection method for a sare thirteen-flavor penniao preparation, which belongs to the technical field of medicine. Background technique [0002] Tibetan medicine is a treasure in my country's medical treasure house, ranking first among the four major ethnic groups in my country (Tibetan, Mongolian, Uyghur, and Dai). It is a summary of Tibetan people's long-term life experience and the process of fighting diseases At the same time as the experience of ethnic medicine, it absorbed the medical theories of traditional Chinese medicine, Dashi, Tianzhu, etc., and gradually formed a complete theoretical system. Tibetan medicine is an important part of the motherland's treasure house of medicine. [0003] The development of Tibetan medicine quality standards in China: Tibetan medicine classics "Jingzhu Materia Medica" and "Sibu Medical Code" describe the classification and morphology in detail, but there is no systematic identificati...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90
Inventor 李晗任松鹏孙绪丁赵延霞艾洛加
Owner JINKE TIBETAN MEDICINE QINGHAI PROV
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