A method for concentrating and recycling polluted acid
A technology of dirty acid and solution, applied in chemical instruments and methods, sulfur trioxide/sulfuric acid, water/sewage multi-stage treatment, etc. Low efficiency and other problems, to achieve the effect of improving the utilization rate of sulfur resources, which is difficult and improves the utilization rate
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Embodiment 1
[0037]A method for concentrating and recycling polluted acid, comprising the following steps:
[0038] Step (1): The first vulcanization: Add the dirty acid solution and sodium sulfide solution with a dosage ratio of 1L:25g into a negative pressure reactor with a pressure of -350Pa and mix evenly, react at 60°C for 40min, and the reaction stops The material in the final negative pressure reactor is transported to the filter press for filtration through the filter press pump, and the filtered filter residue is transported to the batching system for recycling, and the filtrate is transported to the next reactor for the second vulcanization treatment. A small amount of H produced in the process 2 S gas, through the induced draft fan, is sucked into the supporting lye washing tower by the negative pressure of -950~-1000Pa.
[0039] Step (2): The second vulcanization: Add the filtrate and sodium sulfide solution obtained in the step (1) with a dosage ratio of 1L:44g to a negative ...
Embodiment 2
[0046] A method for concentrating and recycling polluted acid, comprising the following steps:
[0047] Step (1): The first vulcanization: Add the dirty acid solution and sodium sulfide solution with a dosage ratio of 1L:10.5g into a negative pressure reactor with a pressure of -250Pa and mix evenly, react at 70°C for 25min, and react After the stop, the material in the negative pressure reactor is transported to the filter press for filtration through the filter press pump, and the filtered filter residue is transported to the batching system for recycling, and the filtrate is transported to the next reactor for the second vulcanization treatment. A small amount of H produced in the process 2 The S gas is sucked into the matching lye washing tower by the negative pressure of -950~-1000Pa through the induced draft fan.
[0048] Step (2): Second vulcanization: Add the filtrate and sodium sulfide solution obtained in step (1) with a dosage ratio of 1L:29g into a negative pressu...
Embodiment 3
[0055] A method for concentrating and recycling polluted acid, comprising the following steps:
[0056] Step (1): The first vulcanization: add the dirty acid solution and sodium sulfide solution with a dosage ratio of 1L:17g into a negative pressure reactor with a pressure of -300Pa and mix evenly, react at 65°C for 32min, and the reaction stops The material in the final negative pressure reactor is transported to the filter press for filtration through the filter press pump, and the filtered filter residue is transported to the batching system for recycling, and the filtrate is transported to the next reactor for the second vulcanization treatment. A small amount of H produced in the process 2 The S gas is sucked into the matching lye washing tower by the negative pressure of -950~-1000Pa through the induced draft fan.
[0057] Step (2): Second vulcanization: Add the filtrate and sodium sulfide solution obtained in step (1) with a dosage ratio of 1L:29g into a negative press...
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