Nutritional anti-inflammatory mouth rinse and preparation method thereof
A gargle and nutrition technology, which is applied to the preparation of nutritional anti-inflammatory gargle, and the field of nutritional anti-inflammatory gargle, can solve the problems of inedible gargle, difficult removal of medicines, damage to oral cavity appearance, etc.
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Embodiment 1
[0026] Step 1, prepare noni fruit extract
[0027] 1.1) Soak fresh Noni fruit with a maturity of 70% to 80% in 1.0mg / L ozone water for 20 minutes, wash twice, filter dry, put it in a closed tank, and ferment naturally at room temperature for 10 days, mash and separate , to obtain water-soluble noni extract and noni pomace;
[0028] 1.2) The Noni pomace obtained above is mashed, and based on the quality of Noni pomace, add 8 times the quality of water and mix, then add 0.1% pectinase, 0.02% lipase, 0.04% Acid protease, hydrolyzed at room temperature for 5 hours, inactivated at 90°C, separated to obtain enzymatic hydrolyzate and residue;
[0029] 1.3) Squeeze the noni residue (many are hard fruits) obtained in 1.2), dry it, grind it, mix it with 50% edible ethanol according to the mass ratio of 1:6, soak it for 24 hours, filter, and the filtrate is at 80± Reflux extraction at 5°C, vacuum concentration and recovery of ethanol; repeated extraction twice, recovery of ethanol, com...
Embodiment 2
[0035] Step 1, prepare noni fruit extract
[0036] 1.1) Soak fresh Noni fruit with a maturity of 70% to 80% in 1.0mg / L ozone water for 20-30 minutes, wash twice, filter dry, put it in a closed tank, and ferment naturally at room temperature for 12 days, then mash it , separated to obtain water-soluble noni extract and noni pomace;
[0037] 1.2) The Noni pomace obtained above is mashed, and based on the quality of Noni pomace, add 9 times the quality of water and mix, then add 0.1% pectinase, 0.02% lipase, 0.04% Acid protease, hydrolyzed at room temperature for 6 hours, inactivated at 90°C, separated to obtain enzymatic hydrolyzate and residue;
[0038] 1.3) Squeeze the noni residue (many are hard fruits) obtained in 1.2), dry it, grind it, mix it with 60% edible ethanol according to the mass ratio of 1:7, soak it for 30 hours, filter, and the filtrate is at 80± Reflux extraction at 5°C, vacuum concentration and recovery of ethanol; repeated extraction twice, recovery of etha...
Embodiment 3
[0044]Step 1, prepare noni fruit extract
[0045] 1.1) Soak fresh noni fruit with a maturity of 70% to 80% in 1.0mg / L ozone water for 20-30 minutes, wash twice, filter dry, put into a closed tank, and ferment naturally at room temperature for 15 days, mash , separated to obtain water-soluble noni extract and noni pomace;
[0046] 1.2) The Noni pomace obtained above is mashed, and based on the quality of Noni pomace, add 10 times the quality of water and mix, then add 0.1% pectinase, 0.02% lipase, 0.04% Acid protease, hydrolyzed at room temperature for 7 hours, inactivated at 90°C, separated to obtain enzymatic hydrolyzate and squeezed residue;
[0047] 1.3) Mix the dried noni residue obtained in 1.2) with 70% edible ethanol at a mass ratio of 1:8, soak for 36 hours, filter, reflux the filtrate at 80±5°C, concentrate in vacuum and recover ethanol; repeat Extract twice, reclaim ethanol, combine filtrate, obtain concentrate;
[0048] 1.4) Combine the above-mentioned water-solu...
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