Photocatalyst LiSm2NbO6 with visible light response and preparation method thereof
A photocatalyst and visible light technology, applied in the field of inorganic photocatalytic materials, can solve the problems of limited types of photocatalysts, low light conversion efficiency, difficult synthesis, etc., and achieve a wide range of visible light response frequency, high light conversion efficiency and simple preparation method. Effect
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Embodiment 1
[0018] (1) 99.9% analytically pure chemical raw material Li 2 CO 3 、Sm 2 o 3 and Nb 2 o 5 The raw powder of LiSm 2 NbO 6 The composition weighs the ingredients.
[0019] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind until fine, take it out and dry it, and pass through a 200-mesh sieve.
[0020] (3) Pre-fire the uniformly mixed powder in step (2) at 950°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then pulverize it with a ball mill to make the average particle diameter smaller than 2 μm, that is, LiSm 2 NbO 6 powder.
[0021] The prepared photocatalyst, under the irradiation of visible light with a wavelength greater than 420nm, can remove 97.5% of methyl orange in 60 minutes.
Embodiment 2
[0023] (1) 99.9% analytically pure chemical raw material Li 2 CO 3 、Sm 2 o 3 and Nb 2 o 5 The raw powder of LiSm 2 NbO 6 The composition weighs the ingredients.
[0024] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind until fine, take it out and dry it, and pass through a 200-mesh sieve.
[0025] (3) Pre-fire the uniformly mixed powder in step (2) at 980°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then pulverize it with a ball mill to make the average particle diameter smaller than 2 μm, that is, LiSm 2 NbO 6 powder.
[0026] The prepared photocatalyst can remove 98.4% of methyl orange in 60 minutes under the irradiation of visible light with a wavelength greater than 420nm.
Embodiment 3
[0028] (1) 99.9% analytically pure chemical raw material Li 2 CO 3 、Sm 2 o 3 and Nb 2 o 5 The raw powder of LiSm 2 NbO 6 The composition weighs the ingredients.
[0029] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind until fine, take it out and dry it, and pass through a 200-mesh sieve.
[0030] (3) Pre-fire the uniformly mixed powder in step (2) at 1000°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then pulverize it with a ball mill to make the average particle diameter smaller than 2 μm, that is, LiSm 2 NbO6 powder.
[0031] The prepared photocatalyst can remove 98.0% of methyl orange in 60 minutes under the irradiation of visible light with wavelength greater than 420nm.
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