A preparation method based on graphene-enhanced flame-retardant recycled polyester staple fiber
A technology of recycled polyester and graphene, applied in the direction of single-component polyester artificial filaments, etc., can solve the problems of poor mechanical properties of recycled polyester fibers, and achieve good spinning shape, excellent fiber quality, and superior electrical conductivity Effect
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Embodiment 1
[0036] (1) Preparation of graphene masterbatch
[0037] Graphene is treated with surface sulfonic acid group functionalization, the particle size of graphene is 500nm~1000nm, graphene and polyvinylpyrrolidone are stirred, mixed and dispersed according to the mass ratio of 2:1 to obtain graphene particles; graphene particles are added In the polyester powder, the addition of graphene particles is 10% of the quality of the polyester powder, and the graphene masterbatch is produced by a twin-screw granulation process;
[0038] (2) Preparation of phosphorus-based halogen-free flame-retardant masterbatch
[0039] The mixture of N-methylolpropionamide methyl phosphonate and dimethyl methyl phosphonate with a particle size of 0.1 ~ 8um is mixed with polyester powder at high speed, and then the phosphorus-containing particles are produced through a screw granulation process. The phosphorus content of the flame retardant masterbatch is 60000ppm;
[0040] (3) According to the mass per...
Embodiment 2
[0046] (1) Preparation of graphene masterbatch
[0047] Graphene is functionalized with surface sulfonic acid groups, and the particle size of graphene is 500nm to 1000nm. According to the mass ratio of 5:1, graphene and tetracyanodimethylbenzoquinone are stirred, mixed and dispersed to obtain graphene particles; Graphene particles are added in the polyester powder, the addition of graphene particles is 15% of the quality of the polyester powder, and the graphene masterbatch is obtained by a twin-screw granulation process;
[0048] (2) Preparation of phosphorus-based halogen-free flame-retardant masterbatch
[0049] Mix hydroxyethylphenylphosphinic acid with a particle size of 0.1-8um and polyester powder at high speed to produce phosphorus-containing particles through a screw granulation process. The phosphorus content of the flame-retardant masterbatch is 100,000ppm;
[0050] (3) According to the mass percentage, take 2% graphene masterbatch, 8% phosphorus-based halogen-fre...
Embodiment 3
[0056] (1) Preparation of graphene masterbatch
[0057] Graphene is treated with surface sulfonic acid group functionalization, the particle size of graphene is 500nm~1000nm, graphene and polyvinyl alcohol are stirred, mixed and dispersed according to the mass ratio of 1:1 to obtain graphene particles; graphene particles are added to In the polyester powder, the addition of graphene particles is 20% of the quality of the polyester powder, and the graphene masterbatch is produced by a twin-screw granulation process;
[0058] (2) Preparation of phosphorus-based halogen-free flame-retardant masterbatch
[0059] Phosphorus-containing granules are produced by mixing reactive phosphorus-based halogen-free flame retardants with polyester powder at high speed, and the phosphorus content of the flame-retardant masterbatch is 80,000ppm;
[0060] (3) Mix and dry graphene masterbatch and phosphorus-based halogen-free flame-retardant masterbatch with recycled polyester raw materials accor...
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