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A kind of high-viscosity asphalt and its preparation method

A high-viscosity asphalt and bitumen technology, applied in the field of petroleum asphalt, can solve problems such as affecting the service life of asphalt pavements affecting the quality of modified asphalt, difficulty in dispersing polymers in asphalt, and incompatibility of asphalt, etc. Wide and simple preparation method

Active Publication Date: 2017-01-18
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the differences in molecular weight, density, viscosity, etc. between most polymer materials and asphalt, it is difficult to disperse the polymer in asphalt, and it is not completely compatible with asphalt, resulting in poor storage stability of the modified asphalt system at high temperature and easy separation. layer, which affects the quality of modified asphalt and the normal construction and service life of asphalt pavement

Method used

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  • A kind of high-viscosity asphalt and its preparation method
  • A kind of high-viscosity asphalt and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Heat the base asphalt A to 150°C until it is molten and flowing, take 100 parts of the base asphalt and send it into the reaction tank, start the agitator, keep the temperature of the reaction tank at 160°C, and add 0.3 parts of polyphosphoric acid into the reaction tank , reacted for 70 minutes at a stirring speed of 2000 rpm, then added 3.0 parts of extender mother liquor, continued high-speed stirring for 60 minutes, and finally added 2.0 parts of vinylbisstearamide (EBS) and 0.3 parts of silane coupling Agent KH-560 was stirred and reacted for 30 minutes to obtain the high-viscosity bitumen of the present invention. The basic properties of the product are shown in Table 2.

Embodiment 2

[0032] Heat base asphalt B to 150°C until it is molten and flowing, take 100 parts of base asphalt and send it into the reaction tank, start the agitator, keep the temperature of the reaction tank at 160°C, add 0.6 parts of polyphosphoric acid into the reaction tank , reacted for 100 minutes at a stirring speed of 2000 rpm, then added 6.0 parts of extender mother liquor, continued high-speed stirring for 60 minutes, and finally added 3.0 parts of vinylbisstearamide (EBS) and 0.2 parts of silane coupling Agent KH-560 was stirred and reacted for 30 minutes to obtain the high-viscosity bitumen of the present invention. The basic properties of the product are shown in Table 2.

Embodiment 3

[0034] Heat the base asphalt A to 150°C until it is molten and flowing, take 100 parts of the base asphalt and send it into the reaction tank, start the agitator, keep the temperature of the reaction tank at 160°C, and add 0.8 parts of polyphosphoric acid into the reaction tank , reacted for 120 minutes at a stirring speed of 2000 rpm, then added 8.0 parts of extender mother liquor, continued high-speed stirring for 60 minutes, then added 0.3 parts of cetyl alcohol, stirred and reacted for 15 minutes, and finally, the reaction tank When the temperature was raised to 165°C, 4.0 parts of vinyl bisstearamide (EBS) and 0.3 parts of silane coupling agent KH-560 were added, and the reaction was stirred for 30 minutes to obtain the high-viscosity bitumen of the present invention. The basic properties of the product are shown in Table 2.

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Abstract

The invention discloses novel high viscosity asphalt and a preparation method thereof. The novel high viscosity asphalt comprises the following raw materials in parts by weight: 100 parts of base asphalt with high asphaltene content, 0.1-1.2 part of polyphosphoric acid, 2-12 parts of a ductility improver mother liquid, 1-8 parts of a dispersant, and 0.2-0.5 part of a coupling agent. The preparation method comprises the following steps: adding the polyphosphoric acid in the molten base asphalt to perform a chemical modification reaction, then adding the ductility improver mother liquid, continuing to react, and finally adding the dispersant and the coupling agent to continue to react for a period of time to prepare high viscosity asphalt, wherein the whole process is performed under a highs-speed stirring condition. The high viscosity asphalt is high in 60-degree dynamic viscosity, high in softening point, high in low-temperature ductility, stable to store, and good in adhesion to aggregates, has excellent high temperature stability, excellent low temperature anti-cracking performance, excellent anti-fatigue performance and excellent water resistance, is especially suitable for high-temperature humid areas, areas with relatively high diurnal temperature difference, and paving of heavy-duty roads and drainable pavements, effectively prevents common pavement damages such as pavement rutting, pavement upheaval, pavement fatigue cracking, pavement cold cracking and water encroachment on pavements, and prolongs the service life of the pavement.

Description

technical field [0001] The invention is suitable for the field of petroleum asphalt, and in particular relates to a high-viscosity asphalt and a preparation method. Background technique [0002] With the increasing traffic volume and axle load and the high temperature in summer, the fluidity damage and channelized traffic on the asphalt pavement caused by the combined effect of high temperature and wheel rolling are becoming more and more serious, and a large number of rutting, wrapping and cracking appear on the asphalt pavement and other damage. Rutting damage on asphalt pavement causes excessive deformation of the pavement, affects the smoothness of the pavement, weakens the strength of the surface layer and the overall structure of the pavement, and induces other pavement diseases. Long-term practice has shown that there is a good correlation between the dynamic viscosity of asphalt materials at 60°C and the strength and rutting resistance of asphalt mixtures at the hig...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L95/00C08L9/06C08L91/00C08K13/02C08K3/32C08K5/20C08K5/05C08K5/5435
Inventor 陈杰徐青柏宣根海石君章万淼
Owner CHINA PETROLEUM & CHEM CORP
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