Mono-ammonium phosphate produced by using wet process phosphoric acid and production method of mono-ammonium phosphate
A technology of monoammonium phosphate and wet-process phosphoric acid, which is applied in the direction of phosphate, phosphorus oxyacid, etc., can solve the problems of reducing the production cost of monoammonium phosphate products, polluting the crop growth environment, and difficult to control impurity content, and achieves the improvement of fluorine content , Improve the effect of purity and quality
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Embodiment 1
[0025] A kind of monoammonium phosphate produced by wet process phosphoric acid, the fluorine content of the monoammonium phosphate is 0.53%.
[0026] The production method of the monoammonium phosphate that this utilizes wet-process phosphoric acid to produce may further comprise the steps:
[0027] (1) Pre-neutralization: place phosphoric acid in the pre-neutralization tank, pass ammonia gas into it, and adopt the method of stirring while passing in, the stirring speed during stirring is 30r / min, and the When the molar ratio of ammonia gas to phosphoric acid is 0.5, continue to maintain the stirring speed for 20 minutes, and carry out heating treatment on the pre-neutralization tank, the heating rate is 0.3 ℃ / min heating treatment, and detect the mixed liquid in the pre-neutralization tank PH value, when the PH value reaches 0.5, stop the heating treatment, and obtain a solid-liquid mixture for use;
[0028] (2) Separation: the solid-liquid mixture obtained in step 1) is pl...
Embodiment 2
[0035] A kind of monoammonium phosphate produced by wet process phosphoric acid, the fluorine content of the monoammonium phosphate is 0.48%.
[0036] The production method of the monoammonium phosphate that this utilizes wet-process phosphoric acid to produce may further comprise the steps:
[0037] (1) Pre-neutralization: Place phosphoric acid in the pre-neutralization tank, pass ammonia gas into it, and adopt the method of stirring while passing in, and the stirring speed during stirring is 50r / min. When the molar ratio of ammonia gas to phosphoric acid is 0.7, continue to maintain the stirring speed for 30 minutes, and carry out the temperature rise treatment on the pre-neutralization tank, and the heating rate is 0.6 °C / min. PH value, when the PH value reaches 0.8, stop the heating treatment, and obtain a solid-liquid mixture for use;
[0038] (2) Separation: the solid-liquid mixture obtained in step 1) is placed in a centrifuge for centrifugation. The rotating speed of ...
Embodiment 3
[0045] A monoammonium phosphate produced by wet process phosphoric acid, the fluorine content of the monoammonium phosphate is 0.68%.
[0046] The production method of the monoammonium phosphate that this utilizes wet-process phosphoric acid to produce may further comprise the steps:
[0047] (1) Pre-neutralization: place phosphoric acid in the pre-neutralization tank, pass ammonia gas into it, and adopt the method of stirring while passing in, and the stirring speed during stirring is 40r / min, and when it is passed into When the molar ratio of ammonia gas to phosphoric acid is 0.6, continue to maintain the stirring speed for 25 minutes, and carry out heating treatment on the pre-neutralization tank, the heating rate is 0.5 ℃ / min heating treatment, and detect the mixed liquid in the pre-neutralization tank PH value, when the PH value reaches 0.7, stop the heating treatment, and obtain a solid-liquid mixture for use;
[0048] (2) Separation: Place the solid-liquid mixture obta...
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