A kind of production method of preparing the special fertilizer of yew by-product of potassium dihydrogen phosphate
A technology of potassium dihydrogen phosphate and its production method, which is applied in the direction of chemical instruments and methods, applications, phosphorus compounds, etc., which can solve problems such as stoppage, soil compaction, and low purity of potassium dihydrogen phosphate, and achieve the effect of good absorption rate
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Embodiment 1
[0069] A kind of production method of preparing potassium dihydrogen phosphate by-product yew special fertilizer provided by this embodiment mainly includes the following steps:
[0070] 1) Mix phosphoric acid and carbonamide at a molar ratio of 1.2:1, heat up from 80°C to 160°C at a heating rate of 6°C / min, stir and react for 4-5 hours, and separate the intermediate; then use the intermediate and The basic potassium salt is mixed according to the molar ratio of 1:1.4, and the pH value is adjusted to 8.5. After the reaction is completed, a slurry containing nitrogen, phosphorus, and potassium is obtained, and the slurry containing nitrogen, phosphorus, and potassium is placed in a cooling crystallizer Lower the temperature to 35-40°C in the middle, carry out crystallization and filtration treatment, and circulate the filtrate in the cooling crystallizer for crystallization treatment, the obtained filter cake is potassium dihydrogen phosphate product, and detect the component co...
Embodiment 2
[0079] A kind of production method of preparing potassium dihydrogen phosphate by-product yew special fertilizer provided by this embodiment mainly includes the following steps:
[0080] 1) Mix phosphoric acid and carbonamide at a molar ratio of 1.5:1, heat up from 80°C to 160°C at a heating rate of 6°C / min, stir and react for 4-5 hours, and separate the intermediate; then use the intermediate and The basic potassium salt is mixed according to the molar ratio of 1:1.1, and the pH value is adjusted to 8.5. After the reaction is completed, a slurry containing nitrogen, phosphorus, and potassium is obtained, and the slurry containing nitrogen, phosphorus, and potassium is placed in a cooling crystallizer Lower the temperature to 35-40°C in the middle, carry out crystallization and filtration treatment, and circulate the filtrate in the cooling crystallizer for crystallization treatment, the obtained filter cake is potassium dihydrogen phosphate product, and detect the component co...
Embodiment 3
[0089] A kind of production method of preparing potassium dihydrogen phosphate by-product yew special fertilizer provided by this embodiment mainly includes the following steps:
[0090] 1) Mix phosphoric acid and carbonamide at a molar ratio of 1.3:1, and raise the temperature from 80°C to 160°C at a heating rate of 6°C / min, stir and react for 4-5 hours, and separate the intermediate; then use the intermediate and The basic potassium salt is mixed according to the molar ratio of 1:1.3, and the pH value is adjusted to 8.7. After the reaction is completed, a slurry containing nitrogen, phosphorus, and potassium is obtained, and the slurry containing nitrogen, phosphorus, and potassium is placed in cooling crystallization Cool the temperature in the device to 35-40°C, carry out crystallization and filtration treatment, and circulate the filtrate in the cooling crystallizer for crystallization treatment, the obtained filter cake is potassium dihydrogen phosphate product, and detec...
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