A kind of preparation method and application of building material additive
A technology of additives and building materials, applied in the direction of botanical equipment and methods, applications, biocides, etc., can solve the problems of loss, no toluene removal effect, high cost, etc.
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Embodiment 1
[0031] Example 1: Preparation of building material additives containing Weizhou Sargassum extract
[0032] Take 100g of Weizhou Sargassum, wash and chop, and prepare according to the following steps:
[0033] (1) Extraction treatment:
[0034] Extract with 30 times of water at a temperature of 100°C, extract 3 times in total, and combine the extracts from 3 times;
[0035] (2) Microwave treatment:
[0036] Carry out microwave treatment to the extract of step (1), radiation time 10min, microwave power 1200W;
[0037] (3) Enzymolysis:
[0038]Concentrate the microwave-treated extract in step (1) under reduced pressure to 1 / 3 of the original volume, and add a compound enzyme preparation composed of cellulase, β-glucanase, and papain at a ratio of parts by weight of 1.2:2.1:1.6 , take it out after 8 hours in a constant temperature water bath at 30°C, put it in -18°C for quick freezing into ice, take it out and let it melt at room temperature, and repeat the quick freezing and ...
Embodiment 2
[0043] Embodiment 2: Preparation of building material additive containing Sargassum Heinzki extract
[0044] Get 100g of Sargassum Heinz, wash and chop, and prepare according to the following steps:
[0045] (1) Extraction treatment:
[0046] Extract with 10 times of 95% ethanol at a temperature of 50°C, extract 3 times in total, and combine the extracts from 3 times;
[0047] (2) Microwave treatment:
[0048] Carry out microwave treatment to the extract of step (1), radiation time 5min, microwave power 800W;
[0049] (3) Enzymolysis:
[0050] Concentrate the microwave-treated extract in step (1) under reduced pressure to 1 / 4 of the original volume, and add a compound enzyme preparation composed of cellulase, β-glucanase, and papain at a ratio of parts by weight of 3.6:5.2:4.5 , take it out after 8 hours in a constant temperature water bath at 30°C, put it in -18°C for quick freezing into ice, take it out and let it melt at room temperature, and repeat the quick freezing a...
Embodiment 3
[0055] Embodiment 3: Effect test of activated water
[0056] Group A: Take 10mL of untreated ordinary tap water, filter it after 10min, centrifuge, take the supernatant to test the water molecules 17 O NMR FWHM (NMRFWHM).
[0057] Group B: 100g of the seaweed extract prepared in Example 1 was made into ultrafine nanoparticles of metal oxides in a supercritical state, and 0.3g of the above ultrafine nanoparticles was added to 10mL tap water, filtered after 10min, and centrifuged. Take the supernatant and test for water molecules 17 O NMR FWHM (NMRFWHM).
[0058] Group C: 100g of the extract prepared in Example 2 was made into ultrafine nanoparticles of metal oxides in a supercritical state, and 0.3g of the above ultrafine nanoparticles were added to 10mL tap water, filtered after 10min, and centrifuged , take the supernatant to test the water molecules 17 O NMR FWHM (NMRFWHM).
[0059] The test instrument is a BruckerAVANCE III 400MHz superconducting nuclear magnetic reson...
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