Method for preparing high specific capacity and low leakage current carbon nanofiber nitrided conductive macromolecule composite material
A technology of carbon nanofibers and conductive polymers, which is applied in the field of carbon materials and chemical power sources, can solve problems such as unknown influences, achieve the effects of increasing nitrogen content, increasing specific capacity, and avoiding irreversible stacking
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[0067] The preparation method of a carbon nanofiber nitrided conductive polymer composite material with high specific capacity and low leakage current provided in this embodiment specifically includes:
[0068] 1) Weigh with JA2003N electronic balance (Shanghai Precision Scientific Instrument Co., Ltd.), the water-soluble carboxylated graphene powder is formulated into suspoemulsion A with a content of 2-3%, and CHJ-1 constant temperature magnetic stirrer (Shanghai Nanhui Telecom Apparatus factory) stir evenly, and equal amount is divided into three parts for subsequent use, and the content of the preferred water-soluble carboxylated graphene of the present embodiment is 2%;
[0069]2) Dissolve polyacrylonitrile (PAN) in N,N-dimethylformamide (DMF), then use high-voltage electrospinning technology to weave PAN precursors, and put the spun PAN precursors in a tubular reactor Carry out carbonization to prepare carbon nanofibers (CNFs), then add carbon nanofibers (CNFs) in 1 part...
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