A composite transparent holographic film production process
A production process and composite technology, applied in the direction of layered products, copying/marking methods, printing, etc., can solve the problems of restricting the research and application of transparent holographic films, diffraction pattern interference, and difficult to control uniformity, so as to avoid structural and Functional compatibility and matching issues, reducing equipment and labor costs, and the effect of reducing equipment and footprint
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Embodiment 1
[0044] A composite transparent holographic film production process, such as figure 1 shown, including the following steps:
[0045] Step 101, preparation of composite coating solution:
[0046] 1) Preparation of nanomaterial dispersion: use tetrahydrofuran as a solvent, ammonium polyacrylate as a dispersant, weigh titanium dioxide with an average particle size of 40nm and add it to tetrahydrofuran, use 6KW power ultrasonic wave, and oscillate at a frequency of 80KHz for 4min to make a uniform Dispersion system; ultrasonic power, frequency and oscillation time can be adjusted according to actual needs, generally use 6-8KW power, 80-100KHz ultrasonic oscillation for 4-8min;
[0047] Dispersion liquid component and content (weight part) proportioning are as follows:
[0048] Tetrahydrofuran 56.7
[0049] Ammonium polyacrylate 32.4
[0050] Nano Titanium Dioxide 10
[0051] The above ratio relationship can make nano-titanium dioxide uniformly dispersed without sedimentation f...
Embodiment 2~5
[0068] The basic production process of the composite transparent holographic film described in Examples 2 to 5 is the same as that of Example 1, the difference mainly lies in the different components and volume fractions of the composite coating solution, as shown in Table 1.
[0069] Table 1: Components and proportioning relationship of the composite coating solution of Examples 1 to 5:
[0070] serial number Nanomaterials (average particle size) Dispersion ratio Polyurethane solution ratio Volume fraction of nanomaterials Composite coating liquid refractive index Composite coating solution light transmittance Example 1 Titanium dioxide (40nm) 8 40 2% 1.56 92% Example 2 Titanium dioxide (50nm) 20 40 5% 1.57 90% Example 3 Zinc oxide (60nm) 40 40 10% 1.63 88% Example 4 Zinc sulfide (50nm) 60 40 15% 1.7 85% Example 5 Cadmium sulfide (60nm) 40 40 10% 1.63 88%
[0071] From the experimental data o...
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