A preparing method of a rare earth catalytic cracking double-metal deactivator
A catalytic cracking, rare earth element technology
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[0037] See Figure 1 to Figure 3 , a kind of preparation method of rare earth element catalytic cracking double metal passivator, concrete steps are:
[0038] A. Mix and stir 300-600kg of mother liquor A, 50-150kg of mother liquor B and 5-20kg of pH regulator;
[0039] B. 30-80kg of deionized water, stirred for 30-60 minutes and discharged.
[0040] The preparation steps of mother liquor A are:
[0041] a. Add 6-20kg of pH regulator, 10-35kg of organic acid, and 20-80kg of organic amine into a 500kg reaction flask, and stir for 10 minutes;
[0042] b. Add 80-120kg of antimony powder, continue to increase the temperature by 80-100℃, add 100-170kg of oxidant dropwise;
[0043] c. Condensation and reflux for 1 to 2 hours,
[0044] d. Add 15-35 kg of stabilizer, stir to cool down to room temperature, and discharge to obtain mother liquor A.
[0045] The preparation steps of mother liquor B are:
[0046] a. Add 100-150kg of rare earth powder, 100-140kg of organic acid, 100-20...
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