Method for indirectly measuring content of uranium in soil through atomic fluorescence spectroscopy
An atomic fluorescence spectrometry and content technology, which is applied in the field of indirect determination of uranium content in soil by atomic fluorescence spectrometry, can solve the problems of interference, inability to directly determine element uranium, and expensive inductively coupled plasma mass spectrometry instruments.
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[0027] The present invention will be further described below in conjunction with specific implementation.
[0028] A method for indirect determination of uranium content in soil by atomic fluorescence spectrometry. The grades of reagents and chemicals used in the method are all analytical pure. The operation steps are as follows:
[0029] 1. Soil pretreatment
[0030] Method 1 wet digestion
[0031] Weigh 1g of soil, accurate to 0.0001g, place it in a 100mL beaker, add HNO with a mass percentage concentration of 58% 3 : 10 mL of a solution of HCl=3:1 with a concentration of 36.5% by mass, and left to stand overnight. Slowly heat until white smoke is emitted, then add 5mL of hydrochloric acid with a concentration of 36.5% by mass, mix well and heat until the remaining solution is 2-3mL, filter while hot, transfer the filtrate into a 25mL volumetric flask after cooling slightly, and dilute with water to scale, and mix well to obtain a digested soil sample solution. Do blank ...
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