Intermediate film for laminated glass, and laminated glass
A technology of laminated glass and interlayer film, applied in glass/slag layered products, layered products, chemical instruments and methods, etc., can solve the problem of large infrared thermal effect, and achieve the effect of improving transmittance and heat insulation.
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Embodiment 1
[0193] (1) Production of interlayer film
[0194] Prepare a 0.19% by weight ethanol solution containing magnesium bis(2-ethylbutyrate) metal salt in an amount of 0.067% by weight in 100% by weight of the obtained interlayer film %.
[0195] Mix 40 parts by weight of triethylene glycol di-2-ethylhexanoate (3GO) with the following materials: CWO particles, so that their amount in the obtained intermediate film 100% by weight is 0.035% by weight; ITO particles , so that its amount in 100% by weight of the obtained interlayer film is 0.14% by weight; a phthalocyanine compound, so that its amount in the obtained interlayer film is 0.004% by weight; After the phosphoric acid ester compound was mixed with a horizontal micro-bead mill, a dispersion was obtained. It should be noted that the content of the phosphate compound was adjusted to be 1 / 10 of the total content of the CWO particles and the ITO particles.
[0196] Add the following substances relative to 100 parts by weight of...
Embodiment 2~10 and comparative example 1~9
[0203] A single-layer interlayer film was produced in the same manner as in Example 1 except that the types and contents of the compounding components were set as shown in Tables 1 and 2 below. The types and compounding amounts of the same polyvinyl butyral resin and plasticizer as in Example 1 were set. Using the obtained interlayer film, laminated glasses A and B including the interlayer film were produced in the same manner as in Example 1.
[0204] In addition, in Comparative Example 7, when compounding the heat ray shielding agent, lanthanum hexaboride particles were compounded so that the amount in the obtained interlayer film was 0.007% by weight. In Comparative Example 8, gallium-doped zinc oxide particles were blended so that the amount in the obtained interlayer film was 0.120% by weight when blending the heat ray shielding agent. In Comparative Example 9, when blending the heat ray shielding agent, an imonium compound ("CIR-RL" manufactured by Nippon Carlit Co., Lt...
Embodiment 11
[0206] (1) Preparation of the first composition for forming the intermediate layer
[0207] Add 60 parts by weight of plasticizer triethylene glycol di-2-ethylhexanoate relative to 100 parts by weight of polyvinyl butyral resin (PVB2), and fully knead with mixing rollers to obtain The first composition of the middle layer.
[0208] (2) Preparation of the second composition for forming the surface layer
[0209] Prepare a 0.19% by weight ethanol solution containing magnesium bis(2-ethylbutyrate) metal salt in an amount of 0.067% by weight in 100% by weight of the obtained interlayer film %.
[0210]Mix 40 parts by weight of triethylene glycol di-2-ethylhexanoate (3GO) with the following materials: CWO particles, so that their amount in the obtained intermediate film 100% by weight is 0.026% by weight; ITO particles , so that its amount in 100% by weight of the intermediate film obtained is 0.127% by weight; a phthalocyanine compound, such that its amount in the obtained inte...
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