Quality detection method for Tibetan medicine composition rheumatism Theron preparation
A technology for rheumatoid sialon solid and preparation, which is applied in the field of medicine, can solve the problems that the quality standard needs to be improved, the quality of main components cannot be effectively controlled, and the quality of this product cannot be controlled comprehensively and accurately, and the product quality is safe and the quality is acceptable. control effect
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Embodiment 1
[0369] Embodiment 1: the quality detection method of Fengshi Sailong Capsules
[0370] Identification:
[0371] (1) Identification of Zicao antler
[0372]Take 10g of the content of Fengshi Sialon Capsules, add 20ml of ethyl acetate, ultrasonically treat for 30 minutes, filter, and concentrate the filtrate to 2ml, and use it as the test solution; take 0.5g of the antler reference medicinal material, and prepare the reference medicinal material solution in the same way Carry out the test according to the Chinese Pharmacopoeia 2010 edition one appendix VIB thin-layer chromatography method, draw each 10 μ L of above-mentioned two kinds of solutions, point respectively on the same silica gel G thin-layer plate, with 5: 5: 0.5: 0.1 xylene-dichloromethane -Acetone-formic acid is used as a developing agent, developed, taken out, dried, and inspected under sunlight respectively; in the chromatogram of the test product, on the position corresponding to the chromatogram of the control ...
Embodiment 2
[0405] Embodiment 2: the quality detection method of Fengshi Sialon Granules
[0406] Identification:
[0407] (1) Identification of Zicao antler
[0408]Take 10g of Rheumatism Sialon Granules, add 20ml of ethyl acetate, ultrasonically treat for 30 minutes, filter, and the filtrate is concentrated to 2ml, as the test solution; take 0.5g of antler reference medicinal material, and prepare the reference medicinal material solution in the same way; Chinese Pharmacopoeia 2010 Edition, Appendix ⅥB thin-layer chromatography test, draw 10 μL of each of the above two solutions, respectively spot on the same silica gel G thin-layer plate, with 5:5:0.5:0.1 xylene-dichloromethane-acetone - Formic acid is used as a developing agent, unfolded, taken out, dried, and inspected under sunlight respectively; in the chromatogram of the test product, on the position corresponding to the chromatogram of the control medicinal material, spots and fluorescent spots of the same color appear;
[0409...
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