A kind of pt/c catalyst for fuel cell and its preparation process
A fuel cell and preparation technology, applied in the field of nanomaterials, can solve the problems of low single output and complicated catalyst process, and achieve the effects of simplifying the process, shortening the preparation time, and enhancing the wettability
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0030] Preparation process of Pt / C catalyst for fuel cell:
[0031] (1) Weigh 1.2g XC-72R carbon black carrier, 150g deionized water, 249g 25g / L ethylene glycol solution of chloroplatinic acid hexahydrate, 90g ethylene glycol, 1M / L Na 2 CO 3 Put 35g of the solution in a 1000mL beaker and stir until the pH of the system is 11 ~ 13;
[0032] (2) The reaction system in step (1) was left to stand for 10 minutes, then ultrasonically stirred for 20 minutes, and then heated by 700W microwave for 10 minutes;
[0033] (3) After the reaction liquid is cooled to room temperature, use H 2 SO 4 Adjust the pH of the system to 4, make the platinum particles settle, and let it stand for 20 minutes;
[0034] (4) Use a filter membrane with a pore size of 1 micron, filter through a positive pressure filter device, wash with 40°C deionized water several times, and finally test the filtrate with 0.1mol / L silver nitrate solution until there is no chloride ion;
[0035] (5) Put the filter cake...
Embodiment 2
[0037] Preparation process of Pt / C catalyst for fuel cell:
[0038] (1) Weigh 1.2g of EC300 carbon black carrier, 180g of deionized water, 249g of 25g / L isopropanol solution of chloroplatinic acid hexahydrate, 70g of isopropanol, and 30g of 1M / L NaOH solution in a 1000mL beaker, and stir until the pH of the system is 11 ~ 13;
[0039] (2) Let the reaction system in step (1) stand for 15 minutes, carry out ultrasonic stirring for 20 minutes, and 800W microwave heating for 7 minutes;
[0040] (3) After the reaction solution is cooled to room temperature, adjust the pH of the system to 3 with HCl to settle the platinum particles and let it stand for 15 minutes;
[0041] (4) Use a filter membrane with a pore size of 1 micron, filter through a positive pressure filter device, wash with deionized water at 30°C several times, and finally test the filtrate with 0.1mol / L silver nitrate solution until there is no chloride ion;
[0042] (5) Put the filter cake in a watch glass and dry...
Embodiment 3
[0044] Preparation process of Pt / C catalyst for fuel cell:
[0045] (1) Weigh 1.2g of EC600 carbon black carrier, 120g of deionized water, 249g of 25g / L pentaerythritol solution of chloroplatinic acid hexahydrate, 50g of pentaerythritol, and 25g of 1M / L Na2CO3 solution in a 1000mL beaker, and stir until the pH of the system is 11 ~ 13;
[0046] (2) The reaction system in step (1) was left to stand for 8 minutes, then ultrasonically stirred for 20 minutes, and then heated by 1000W microwave for 6 minutes;
[0047] (3) After the reaction liquid is cooled to room temperature, adjust the pH of the system to 3 with HNO3 to settle the platinum particles and let it stand for 25 minutes;
[0048] (4) Use a filter membrane with a pore size of 1 micron, filter through a positive pressure filter device, wash with deionized water at 50°C several times, and finally check the filtrate with 0.1mol / L silver nitrate solution until there is no chloride ion;
[0049] (5) Put the filter cake i...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com