Visible light response photocatalyst SrLa10V4O26 and preparation method thereof
A photocatalyst and visible light technology, applied in chemical instruments and methods, physical/chemical process catalysts, metal/metal oxide/metal hydroxide catalysts, etc., can solve poor stability, low photoconversion efficiency, and no visible light response Photocatalytic performance and other issues, to achieve the effect of low cost, simple preparation method and excellent catalytic performance
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Embodiment 1
[0018] (1) 99.9% analytically pure chemical raw material SrCO 3 , La 2 o 3 and V 2 o 5 , by SrLa 10 V 4 o 26 Chemical formula weighing ingredients.
[0019] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind until fine, take it out and dry it, and pass through a 200-mesh sieve.
[0020] (3) Pre-fire the uniformly mixed powder in step (2) at 850°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then use ball mill pulverization to make the particle diameter smaller than 2 μm, that is, to obtain SrLa 10 V 4 o 26 powder.
[0021] The prepared photocatalyst can remove 98.8% of methyl orange in 120 minutes under the irradiation of visible light with a wavelength greater than 420nm.
Embodiment 2
[0023] (1) 99.9% analytically pure chemical raw material SrCO 3 , La 2 o 3 and V 2 o 5 , by SrLa 10 V 4 o 26 Chemical formula weighing ingredients.
[0024] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind until fine, take it out and dry it, and pass through a 200-mesh sieve.
[0025] (3) Pre-fire the uniformly mixed powder in step (2) at 870°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then use a ball mill to make the particle diameter smaller than 2 μm, that is, to obtain SrLa 10 V 4 o 26 powder.
[0026] The prepared photocatalyst, under the irradiation of visible light with a wavelength greater than 420nm, can remove 99.1% of methyl orange within 120 minutes.
Embodiment 3
[0028] (1) 99.9% analytically pure chemical raw material SrCO 3 , La 2 o 3 and V 2 o 5 , by SrLa 10 V 4 o 26 Chemical formula weighing ingredients.
[0029] (2) Mix the raw materials prepared in step (1), put them into a ball mill jar, add zirconia balls and absolute ethanol, ball mill for 8 hours, mix and grind until fine, take it out and dry it, and pass through a 200-mesh sieve.
[0030] (3) Pre-fire the uniformly mixed powder in step (2) at 880°C, keep it warm for 6 hours, cool it down to room temperature naturally, and then use a ball mill to reduce the particle diameter to less than 2 μm to obtain SrLa 10 V 4 o 26 powder.
[0031] The prepared photocatalyst can remove 98.3% of methyl orange in 120 minutes under the irradiation of visible light with a wavelength greater than 420nm.
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