Compounds for electronic devices
A technology of compounds and atoms, applied in the field of compounds of formula, can solve the problems of limiting the life and efficiency of organic electroluminescence devices
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0223] 2,4,6-Trimethyl-N,N,N',N',N'',N''-hexaphenylbenzene-1,3,5-triamine
[0224]
[0225] 14.0 ml (14 mmol) of 1M tri-tert-butylphosphine in toluene, 1.6 g (7 mmol) of palladium(II) acetate, and then 103.0 g (1.1 mol) of sodium tert-butoxide were added sequentially to 85.0 g (238 mmol) of 1 , 3,5-tribromo-2,4,6-trimethylbenzene [608-72-0] and 161.2g (953mmol) of diphenylamine in a solution of 2000ml of toluene. The reaction mixture was heated to reflux for 16 hours, allowed to cool to 60 °C, 20 ml of acetic acid and 250 ml of water were added, the mixture was allowed to cool to room temperature, the aqueous phase was separated, the organic phase was washed once with 500 ml of water and washed with 500 ml of saturated sodium chloride solution Wash once, then remove toluene under vacuum. The residue was washed by boiling once with 1000 ml of ethanol, dried in vacuo and then recrystallized six times from DMF (about 5 ml / g). Then in high vacuum (p about 10 -6 mbar, T about...
PUM
Property | Measurement | Unit |
---|---|---|
thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com