Process for preparing probe for monitoring water quality of bionic coating containing phospholipid polymers in real time
A real-time monitoring and preparation technology, which is applied to paints, coatings, and test water containing biocide, can solve problems such as the diffusion of toxic substances, adverse effects on the ecological balance of water bodies, and non-compliance with environmental concepts, and achieve low cost and restraint. Biofouling problem, effect of good bacteriostatic properties
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Embodiment 1
[0030] 1. Mix 3g of 2-methacryloyloxyethylphosphorylcholine (MPC) with 7g of butyl methacrylate (BMA) to prepare a solution, and add azobisisobutyronitrile (AIBN) into the solution as a polymerization initiator The polymerization reaction was carried out at 65° C. and argon was used as the protective gas. The polymerization product was precipitated and separated with ether solvent, and dried in vacuum for 24 hours to obtain PMB solid.
[0031] 2. Take 1.00 g of the PMB polymer obtained in the above steps, and prepare it into a 1% ethanol solution by mass percentage.
[0032] 3. Take a water quality monitoring probe and clean it with ultrasonic cleaning. Immerse the probe in the polymer solution for 30 minutes and take it out. After the solvent evaporates, clean the probe with absolute ethanol and distilled water, and dry it in nitrogen.
Embodiment 2
[0034] 1. Synthesize PMB according to the method in Example 1 and be prepared with a 1% aqueous solution by mass fraction, place the semipermeable membrane material in the polymer solution and soak it for 30min, then take it out, and in a 3% sodium chloride solution by mass fraction Preserve by soaking in medium. During use, the semi-permeable membrane material can be processed into a shape suitable for the probe, and then covered and fixed on the surface of the probe.
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