Method for preparing ZnO/Ag nanometer composite materials in room temperature
A nano-composite material and room temperature technology, applied in the field of preparing ZnO/Ag nano-composite materials, can solve problems such as harsh conditions and complex processes, and achieve the effects of easy control of the process, simple process, and easy control of the product
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Embodiment 1
[0019] (1) Take 0.8g of nano-zinc powder that has been ground for 5 hours, disperse it in 34ml (water:cyclohexane=17:1) dispersion system, and shake evenly;
[0020] (2) At room temperature, place the reaction system in (1) in a 40KHz sonicator for 6 hours, during which time take out the Erlenmeyer flask and shake vigorously for 30 seconds every 15 minutes; after the treatment, take out the upper milky white suspension for later use;
[0021] (3) Add dropwise 0.1mol / L AgNO to the milky white suspension in (2) 3 solution until the brown-black flocs no longer increase;
[0022] (4) Centrifuge to separate the brown-black precipitate, and wash it with distilled water to remove the Ag inside + and NO 3 - For impurity ions, repeat this step, and finally place the precipitate in a clean reagent bottle;
[0023] (5) Add absolute ethanol to the reagent bottle obtained in step (4), shake to disperse the precipitate evenly, and place it in an ultrasonic machine for ultrasonic dispers...
Embodiment 2
[0026] (1) Get 1.0g of nano-zinc powder ground for 5h, disperse it in 40ml (water:cyclohexane=19:1) dispersion liquid, shake evenly;
[0027] (2) At room temperature, place the reaction system in (1) in a 40KHz sonicator for 8 hours. During this period, take out the Erlenmeyer flask and shake vigorously for 30 seconds every 15 minutes; after the treatment, take out the upper milky white suspension for later use;
[0028] (3) Add a certain amount of 0.1mol / L AgNO dropwise to the milky white suspension in (2) 3 solution until the brown-black flocs no longer increase;
[0029] (4) Centrifuge to separate the brown-black precipitate and wash it with distilled water to remove the Ag inside + and NO 3 - For impurity ions, repeat this step, and finally place the precipitate in a clean reagent bottle;
[0030] (5) Add absolute ethanol to the reagent bottle obtained in step (4), shake to disperse the precipitate evenly, and place it in an ultrasonic machine for ultrasonic dispersion...
Embodiment 3
[0033] (1) Take 1.2g of nano-zinc powder that has been ground for 5 hours, disperse it in 44ml (water:cyclohexane=21:1) dispersion system, and shake it evenly;
[0034] (2) At room temperature, place the reaction system in (1) in a 40KHz sonicator for 10 hours. During this period, take out the Erlenmeyer flask and shake vigorously for 30 seconds every 15 minutes; after the treatment, take out the upper milky white suspension for later use;
[0035] (3) Add a certain amount of 0.1mol / L AgNO dropwise to the milky white suspension in (2) 3 solution until the brown-black flocs no longer increase;
[0036] (4) Centrifuge to separate the brown-black precipitate and wash it with distilled water to remove the Ag inside + and NO 3 - For impurity ions, repeat this step, and finally place the precipitate in a clean reagent bottle;
[0037] (5) Add absolute ethanol to the reagent bottle obtained in step (4), shake to disperse the precipitate evenly, and place it in an ultrasonic machi...
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