Additive for thermal insulation paint and preparation method, and water-based paint containing additive
A technology of thermal insulation coatings and additives, applied in the direction of coatings, etc., can solve problems such as poor thermal insulation effect, and achieve the effects of good performance, cost reduction and simple process
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[0019] The present invention also provides a method for preparing an additive for heat-insulating coatings, the method comprising the following steps:
[0020] S1. Preparation of microcapsule vitrified microbeads: the phase change energy storage material is infiltrated into the interior of vitrified microbeads by vacuum infiltration method to form the precursor of microcapsule vitrified microbeads; then the precursor is placed in acrylic acid and the first nanometer dioxide Microcapsule vitrified microbeads can be obtained by immersing in the emulsion formed by silicon;
[0021] S2. Preparation of additives: Add dispersant, modifier, thickener, and defoamer into water to fully disperse, then add microcapsules, vitrified microbeads, stir and mix, and finally add nano-oxides and mix to obtain additives for heat-insulating coatings .
[0022] Preferably, the weight ratio of the waved microbeads, phase change material and emulsifier is 3-6:5-10:5-10. The phase change material an...
Embodiment 1
[0030] 1. Preparation of microcapsule wave microbeads: the vitrified microbeads with a particle size of 15um are used to infiltrate the phase change material into the vitrified microbeads by vacuum impregnation method. Heat emulsification in a mixer at a heating temperature of 60°C, and then add vitrified microbeads with a particle size of 15um according to the weight ratio of phase change energy storage material and corrugated microbeads at a ratio of 5:3, at a vacuum degree of 120KPa After fully stirring under the same conditions, filter and dry at room temperature. Then the above-mentioned vitrified microbeads are added to the emulsifier according to the weight ratio of the emulsifier to the waved microbeads in a ratio of 5:4, and the emulsifier is 20 parts of acrylic acid and 10 parts of nano silicon dioxide The emulsion, the particle size of nano silicon dioxide is 20nm. Finally, stir at 1200 rpm for 2 hours, filter, and dry at 120° C. for 2 hours to obtain the above-men...
Embodiment 2
[0044] 1. Prepare microcapsule vitrified microbeads A2 according to the method of Example 1, the difference is: the particle diameter of the waved microbeads is 20um; the weight ratio of the waved microbeads, phase change energy storage material and emulsifier is 6 : 10:10; the emulsifier is an emulsion of 10 parts of acrylic acid and 5 parts of nano-silica, and the particle size of nano-silica is 10nm.
[0045] 2. Prepare additive sample B2 according to the method of Example 1, the difference is that each substance and its content are as follows
[0046] nano-SiO 2 3%
[0047] Nano-TiO 2 1.5%
[0048] Nano ZnO 2 1%
[0049] Microcapsule Vitrified Beads 40%
[0050] BYK 5040 0.25%
[0051] BYK 5027 0.3%
[0052] KH-550 0.45%
[0053] Thickener 0.15%
[0054] Defoamer 0.20%
[0055] water balance
[0056] 3. Prepare water-based paint C2 according to the method of Example 1, the difference is that the weight ratio of additives to water-based paint is 7:13. ...
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