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Test method of children Celandine and fritillary bulb cough syrup

A technology of cough syrup and detection method, which is applied in the directions of measuring devices, instruments, scientific instruments, etc., can solve the problems of incomplete detection methods and the like

Inactive Publication Date: 2013-04-03
吉林草还丹药业有限公司
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Problems solved by technology

[0010] The present invention provides a detection method for the active ingredients of Xiaoerbaibei cough syrup to solve the problem of incomplete detection methods existing in current detection methods

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0021] Xiaoer Baibei cough syrup is produced by Jilin Caohuandan Pharmaceutical Co., Ltd. according to the prescription and process in the background technology.

[0022] Including the following identification methods and content determination methods:

[0023] (1) Identification method

[0024] Take 5ml of this product, children's Baibei cough syrup, add 20ml of ethanol, shake, filter, concentrate the filtrate to nearly dry, add 2ml of ethanol to dissolve, and use it as the test solution; take 2g of celandine reference medicinal material, and make the same method as the reference medicinal material Solution; according to the Chinese Pharmacopoeia 2010 edition, appendix VI B thin-layer chromatography test, draw 2 μl of each of the above two solutions, respectively spot on the same silica gel G thin-layer plate, with n-butanol: glacial acetic acid: water = 7:2 : 1.5 is developing agent, develops, takes out, dries, puts inspection under 365nm ultraviolet lamp, in test sa...

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Abstract

The invention relates to a test method of effective ingredients of a children Celandine and fritillary bulb cough syrup, and belongs to the field of traditional Chinese medicine modernization. Through establishing identification and content determination of the monarch drug Celandine, the method has the advantages that the test method of the children Celandine and fritillary bulb cough syrup is normalized, the components of the monarch drug can be tested more comprehensively to know the content and stability thereof, which is also beneficial to explaining the pharmaceutical material basis of the drug.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicine modernization, and in particular relates to a detection method for children's Baibei cough syrup. Background technique [0002] The composition of traditional Chinese medicine is complex, especially the compound prescription of traditional Chinese medicine often contains many kinds and many kinds of ingredients, forming a very complicated system. At present, the research and development of new effective parts of traditional Chinese medicine preparations and modern compound Chinese medicine preparations are increasing, and new processes and various extraction methods are used in the research and production of medicines. [0003] With the rapid development of modern analysis and testing technology, equipment and instruments, the content determination and chromatographic identification of traditional Chinese medicine have become important means of detection. However, at present, only the ...

Claims

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Application Information

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IPC IPC(8): G01N30/02G01N30/90
Inventor 郭春林徐德辉曹恩辉李坤刘微朱秀峰王晶博马伟才高艳辉刘瑞宝
Owner 吉林草还丹药业有限公司
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