Method for producing coagulant aid through utilizing cow dung
A technology of coagulation aid and cow dung, which is applied in the direction of flocculation/sedimentation water/sewage treatment, etc., which can solve the problems of high cost and small production scale.
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Embodiment 1
[0018] Prepare the coagulant as follows:
[0019] (1) Air-drying and digestion of cow dung: air-dry the collected fresh cow dung and crush it into powder, then place the dry cow dung powder in 20% hydrochloric acid solution, and stir for 10 minutes;
[0020] (2) Modification of cow dung: first soak the cow dung treated in step (1) in a triethylamine solution with a pH of 13 for 40 minutes, and then place the soaked cow dung in a modification solution at 45 degrees Celsius , the modification reaction time is 90 minutes, and the modification solution is 1% acrylic acid solution;
[0021] (3) Removal of solid residues: first sieve the above liquid with a 100μm sieve to remove large particles of debris; then use a 30μm filter membrane to filter;
[0022] (4) Adjustment of pH value: using sodium acetate to adjust the pH of the liquid obtained in step (3) to 6-7;
[0023] (5) Sealing and storage: Add 50ppm formaldehyde, then seal it in a plastic container, and store it in a cool p...
Embodiment 2
[0027] Prepare the coagulant as follows:
[0028] (1) Air-drying and digestion of cow dung: Air-dry the collected fresh cow dung and crush it into powder, then place the dried cow dung powder in 20% hydrochloric acid solution, and stir for 15 minutes;
[0029] (2) Modification of cow dung: First, soak the cow dung treated in step (1) in a triethylamine solution with pH 13 for 30-40 minutes, and then place the soaked cow dung in a modified place at 50 degrees Celsius. In the solution, the modification reaction time is 70 minutes, and the modification solution is 1% acryloyl ester solution;
[0030] (3) Removal of solid residues: first sieve the above liquid with a 100μm sieve to remove large particles of debris; then use a 30μm filter membrane to filter;
[0031] (4) Adjustment of pH value: using sodium acetate to adjust the pH of the liquid obtained in step (3) to 6-7;
[0032] (5) Sealing and storage: Add 50ppm formaldehyde, then seal it in a plastic container, and store it...
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