Method for producing xylose by use of xylose mother liquid
A technology of xylose mother liquor and xylose, which is applied in the direction of sugar derivatives, sugar derivatives, sugar derivatives preparation, etc., can solve the problems of high cost, high cost of xylose, difficult xylose crystallization and purification, and achieve an increase in crystallization rate , the effect of reducing production costs
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Embodiment 1
[0014] Example 1 Production of high-purity xylose by using xylose mother liquor
[0015] 1.1 Preparation of ionizing liquid and xylose mother liquor
[0016] Using 300kg corncobs as raw material, add dilute sulfuric acid at a solid-to-liquid ratio of 1:5 (weight to volume ratio, kg / L), with a sulfuric acid concentration of 1.0%, and keep warm at 120°C for 2.5 hours. After the reaction, centrifuge to obtain a xylose hydrolyzate, then add calcium carbonate to the hydrolyzate to neutralize and adjust the pH to 3, stir for 15 minutes, and filter after standing for 30 minutes to obtain 1380 L of xylose neutralization solution.
[0017] After the xylose neutralizing solution is warmed up to 60°C, add 0.1% powdered activated carbon (weight to volume ratio kg / L), stir for 15 minutes, and filter after 30 minutes of heat preservation to obtain a decolorizing solution with a light transmittance of 5%; the decolorizing solution is sequentially After the cation exchange column 001*7 and t...
Embodiment 2
[0025] Example 2 Utilize xylose mother liquor to produce high-purity xylose
[0026] The preparation of the clutch liquid and the xylose mother liquor is the same as in Example 1.
[0027] In the xylose mother liquor of 20kg (dry matter concentration 63% in the mother liquor, xylose concentration 36%, glucose concentration 10%, arabinose concentration 13%, polysaccharide concentration 4%), add the xylose separation liquid of 200kg (in separation liquid Dry matter concentration 4.6%, xylose concentration 4.0%, glucose concentration 0.24%, arabinose concentration 0.32%, polysaccharide concentration 0.046%), stirring for 15 minutes, obtaining dry matter concentration is 220kg of mixed sugar liquid of 9.0%, and the light transmittance of sugar liquid is 35%.
[0028] Pass the mixed sugar solution through an organic membrane with a molecular weight cut-off of 0.2kD to obtain 231 kg of membrane filtrate, the dry matter concentration of the filtrate is 7.2%, the light transmittance ...
Embodiment 3
[0030] Example 3 Production of high-purity xylose by using xylose mother liquor
[0031] The preparation of the clutch liquid and the xylose mother liquor is the same as in Example 1.
[0032] In the xylose mother liquor of 20kg (dry matter concentration 63% in the mother liquor, xylose concentration 36%, glucose concentration 10%, arabinose concentration 13%, polysaccharide concentration 4%), add the xylose separation liquid of 50kg (in separation liquid Dry matter concentration 4.6%, xylose concentration 4.0%, glucose concentration 0.24%, arabinose concentration 0.32%, polysaccharide concentration 0.046%), stirring for 15 minutes, obtaining dry matter concentration is 70kg of mixed sugar solution of 21.3%, and the light transmittance of sugar solution is 27%.
[0033] Pass the mixed sugar solution through an organic membrane with a molecular weight cut-off of 0.4kD to obtain 73.5 kg of membrane filtrate, the dry matter concentration of the filtrate is 19.3%, the light trans...
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