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Method for identifying millet wine storage time based on multi-electrode sensing technology

A sensing technology and multi-electrode technology, applied in the field of rice wine age identification based on multi-electrode sensing technology, can solve the problems of affecting the detection effect, cumbersome steps, weakening sample differences, etc., so as to overcome incomprehensibility and overcome limitations. , the effect of improving detection sensitivity and accuracy

Active Publication Date: 2013-01-16
JIANGSU UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The application number is 200510050865.X, "An Electrochemical and Signal Analysis and Processing Method for Rice Wine Classification", the patent needs to prepare a mixed solution of rice wine and sodium hydroxide, and the steps are cumbersome
In addition, rice wine and sodium hydroxide will react, which will affect the signal obtained by the electrode from the rice wine sample itself, weaken the difference between samples, and thus affect the detection effect
The composition information of rice wine is complex, and the information of the rice wine sample obtained by using a single electrode in this patent is not sufficient
The application number is 201110203695.X, "a method for detecting the wine age of yellow rice wine". This patent uses six working electrodes, and needs to combine the pH, conductivity and total sugar of rice wine for qualitative analysis of the wine age of rice wine. The extracted There are many eigenvalues, and the steps are more cumbersome

Method used

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  • Method for identifying millet wine storage time based on multi-electrode sensing technology
  • Method for identifying millet wine storage time based on multi-electrode sensing technology
  • Method for identifying millet wine storage time based on multi-electrode sensing technology

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[0018] (1) Such as figure 1 , The present invention uses silver / silver chloride as the reference electrode 5, platinum wire as the counter electrode 4, glassy carbon electrode 1, gold electrode 2 and platinum electrode 3 as working electrodes to form a multi-electrode sensor array system; The electrochemical potentiostat is connected; through the computer, the analog signal is converted into a digital signal through A / D conversion, and the curve of each working electrode scanning yellow wine is obtained; after the characteristic extraction of the curve, data analysis is performed.

[0019] (2) The tested rice wines are rice wines of 4 different years under the "Danyang" brand, which are 3, 5, 8 and 10 years old. There are 30 samples for each rice wine, a total of 120 samples.

[0020] (3) Take 10 mL of rice wine sample 6 in the electrochemical detection cell, insert the multi-electrode sensor array into the rice wine sample, and perform electrochemical cyclic voltammetry scanning t...

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Abstract

The invention discloses a method for identifying the millet wine storage time based on a multi-electrode sensing technology. The method comprises the following steps of: (1) forming a multi-electrode sensing array system by taking silver or silver chloride as a reference electrode, a platinum wire as a pair electrode and a glass carbon, gold or platinum electrode as a working electrode, wherein the electrodes are connected with an electrochemical constant potential rectifier; (2) putting a millet wine sample into an electrochemical detection pool, inserting the electrode array into the sample, and performing electrochemical cyclic volt-ampere scanning, wherein the scanning range is -0.5 to 1.6V, the starting potential and the end potential are -0.5V, and the scanning rate is 0.05 to 0.2V / s; (3) respectively extracting characteristic values of a cyclic volt-ampere curve of the millet wine sample tested by the glass carbon, gold or platinum electrode; and (4) performing standardized preprocessing on the extracted characteristic values, and performing judgment analysis on the characteristic property of the millet wine by a chemical metrology method. By the method, the experiment steps are simplified; and the sensitivity, the reliability and the repetitiveness are greatly improved.

Description

Technical field [0001] The invention relates to a method for detecting the quality of rice wine using multi-electrode sensing technology, in particular to a method for identifying the age of rice wine using multi-electrode sensing technology. Background technique [0002] Rice wine is the oldest wine in my country’s history and one of the world’s three major brewing wines (rice wine, wine and beer). In the process of rice wine brewing, due to the influence of many factors such as raw material varieties, saccharification starter types, brewing methods, brewing seasons, geographical (environmental) conditions, etc., there are many types of rice wine with different flavors and aroma characteristics. In order to assess the quality level and pros and cons of rice wine and promote it to the society for consumers to choose, it is necessary to carry out scientific testing and evaluation on the quality of rice wine. [0003] The content of the quality evaluation of rice wine is mainly phys...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/27
Inventor 陈全胜欧阳琴赵杰文
Owner JIANGSU UNIV
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