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Method for preparing magnetic photonic crystal on basis of biological templates of single scales of butterfly wing

A technology of magnetic photonic crystals and butterfly wings, which is applied in the field of material science, can solve the problems of in-depth research and mastery of the laws of limiting optical properties, and the research and application of limiting optical nano-devices, so as to achieve good controllability, improve response performance, and process simple effect

Active Publication Date: 2012-12-26
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The functional materials prepared from the whole butterfly limit the in-depth study and mastery of its optical properties
The preparation of a single functional material of scales is a delicate and challenging task, which greatly limits the research and application of optical nanodevices.

Method used

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  • Method for preparing magnetic photonic crystal on basis of biological templates of single scales of butterfly wing
  • Method for preparing magnetic photonic crystal on basis of biological templates of single scales of butterfly wing

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] The method for preparing a magnetic photonic crystal based on a single scale biological template of a butterfly wing includes the following steps:

[0031] The first step is to put the butterfly wings into 40wt% CH 3 After 4 hours in the COOH solution, dissolve the minerals that are not easily removed by sintering, then rinse with distilled water and dry for use.

[0032] The second step is the preparation of the precursor solution. FeCl 3 Solution preparation scheme: Under the condition of a hot water bath, prepare a ferric chloride ethanol solution with a concentration of 0.1 mol / L.

[0033] The third step is to put the processed butterfly wings into the prepared precursor solution and soak for 12 hours

[0034] In the fourth step, after the soaking, the sample was taken out, rinsed with distilled water, and then placed in an oven for 10 hours at a temperature of 50°C.

[0035] Step 5: With the help of a microscope, select a single scale with a nickel needle, place it on the s...

Embodiment 2

[0041] The method for preparing a magnetic photonic crystal based on a single scale biological template of a butterfly wing includes the following steps:

[0042] The first step is to put the butterfly wings into 40wt% CH 3 After 4 hours in the COOH solution, dissolve the minerals that are not easily removed by sintering, then rinse with distilled water and dry for use.

[0043] The second step is the preparation of the precursor solution. FeCl 3 Solution preparation scheme: Under the condition of a hot water bath, prepare a ferric chloride ethanol solution with a concentration of 0.1 mol / L.

[0044] The third step is to put the processed butterfly wings into the prepared precursor solution and soak for 20 hours

[0045] In the fourth step, after the immersion, the sample was taken out, rinsed with distilled water, and then placed in an oven for 10 hours at a temperature of 60°C.

[0046] Step 5: With the help of a microscope, select a single scale with a nickel needle, place it on the...

Embodiment 3

[0050] The method for preparing a magnetic photonic crystal based on a single scale biological template of a butterfly wing includes the following steps:

[0051] The first step is to put the butterfly wings into 40wt% CH 3 After 4 hours in the COOH solution, dissolve the minerals that are not easily removed by sintering, then rinse with distilled water and dry for use.

[0052] The second step is the preparation of the precursor solution. FeCl 3 Solution preparation scheme: Under the condition of a hot water bath, prepare a ferric chloride ethanol solution with a concentration of 1mol / L.

[0053] The third step is to put the processed butterfly wings into the prepared precursor solution and soak for 48 hours

[0054] In the fourth step, after the soaking is over, the sample is taken out, rinsed with distilled water, and then placed in an oven to dry for 10 hours at a temperature of 80°C.

[0055] Step 5: With the help of a microscope, select a single scale with a nickel needle, place ...

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Abstract

The invention relates to a method for preparing a magnetic photonic crystal on the basis of biological templates of single scales of a butterfly wing. The method comprises the steps of: carrying surface pretreatment on a whole butterfly biological template; preparing a precursor metal-sol gel solution; placing the treated biological template in the prepared precursor solution for soaking treatment; after the soaking, taking out a sample, flushing by distilled water and drying; under the help of a microscope, selecting soaked single scales and drying by using a drying oven; roasting to remove the biological templates of the single scales to obtain a single butterfly scale ferric oxide material keeping a photonic crystal structure; and further sintering and reducing under hydrogen-argon mixed gas to obtain a single butterfly scale magnetic ferroferric oxide material keeping the photonic crystal structure. The prepared single butterfly scale magnetic material with the natural photonic crystal structure has good response to magnetism and light, can be controlled within a scale range from nanometer to micrometer and has a potential application prospect in the field of magneto-optical communication devices.

Description

Technical field [0001] The invention belongs to the field of materials science, and in particular relates to a method for preparing magnetic photonic crystals based on a single butterfly wing scale biological template. Specifically, it relates to a single butterfly scale using a secondary sintering method to prepare a single material. Flake magnetic photonic crystal method. Background technique [0002] Since the concept of photonic crystal was put forward, it has attracted widespread attention. Because of its special properties that can regulate light, it has potential applications in communications, optical transmission, and nanodevices. [0003] The preparation of photonic crystals that can regulate light in the visible light range is still a very expensive and challenging task under the current experimental technical conditions. The difficulty lies in the preparation of periodic, tens of nanometer to micrometer size structures. And this kind of structure exists widely in natu...

Claims

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Application Information

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IPC IPC(8): C01G49/08B22F9/22
Inventor 朱申敏彭文红张荻陈羽顾佳俊
Owner SHANGHAI JIAO TONG UNIV
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