Preparation method of modified fly ash adsorbent used in phosphorous-containing waste water treatment
A waste water treatment, fly ash technology, applied in the environmental field, can solve problems such as ecological environment loss, water ecological imbalance, etc., and achieve low production cost, safe and simple, economical and simple effects
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Embodiment 1
[0018] A preparation method of a modified fly ash adsorbent for phosphorus-containing wastewater treatment:
[0019] 1) Mix fly ash and sodium hydroxide solution with a molar concentration of 1 mol / L at a solid-to-liquid weight ratio of 1:2, slowly pour the mixture into the reactor, and react at 100°C for 48 hours.
[0020] 2) The reaction product was washed with deionized water and dried at 80°C.
[0021] 3) The dried powder and the sulfuric acid solution with a molar concentration of 2 mol / L were mixed evenly at a solid-liquid weight ratio of 1:2, and stirred and reacted at room temperature for 2 hours;
[0022] 4) After cleaning the mixed liquid in step 3) with deionized water, dry it at 80°C to obtain the treated fly ash powder.
[0023] 5) The treated fly ash powder and polyaluminum chloride are uniformly mixed in a weight ratio of 1000:6 to obtain a modified fly ash adsorbent.
[0024] 6) Take 10 grams of the prepared modified fly ash adsorbent to treat 1000g phosphoru...
Embodiment 2
[0026] A preparation method of a modified fly ash adsorbent for phosphorus-containing wastewater treatment:
[0027] 1) Mix fly ash and sodium hydroxide solution with a molar concentration of 2 mol / L at a solid-to-liquid weight ratio of 1:10, slowly pour the mixture into the reactor, and react at 120°C for 30 hours.
[0028] 2) The reaction product was washed with deionized water and dried at 80°C.
[0029] 3) Mix the dried powder with a sulfuric acid solution with a molar concentration of 5 mol / L according to a solid-to-liquid weight ratio of 1:1, and stir and react at room temperature for 5 hours;
[0030] 4) After cleaning the mixed liquid in step 3) with deionized water, dry it at 80°C to obtain the treated fly ash powder.
[0031] 5) The treated fly ash powder and calcium oxide are uniformly mixed in a weight ratio of 1000:1 to obtain a modified fly ash adsorbent.
[0032] 6) Take 10 grams of the prepared modified fly ash adsorbent to treat 2000 g of phosphorus-containi...
Embodiment 3
[0034] A preparation method of a modified fly ash adsorbent for phosphorus-containing wastewater treatment:
[0035] 1) Mix fly ash and sodium hydroxide solution with a molar concentration of 5 mol / L at a solid-to-liquid weight ratio of 1:1, slowly pour the mixture into the reactor, and react at 180°C for 8 hours.
[0036] 2) The reaction product was washed with deionized water and dried at 80°C.
[0037] 3) The dried powder and the sulfuric acid solution with a molar concentration of 1mol / L are mixed evenly at a solid-to-liquid weight ratio of 1:10, and stirred and reacted at room temperature for 1 hour;
[0038] 4) After cleaning the mixed liquid in step 3) with deionized water, dry it at 80°C to obtain the treated fly ash powder.
[0039] 5) The treated fly ash powder and magnesium oxide are uniformly mixed in a weight ratio of 1000:9 to obtain a modified fly ash adsorbent.
[0040] 6) Take 10 grams of the prepared modified fly ash adsorbent to treat 1500 g of phosphorus-...
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