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A kind of emulsifier for emulsion explosive and preparation method thereof

A technology of emulsified explosives and emulsifiers, which is applied in the direction of non-explosive/non-thermal agent components, explosives, offensive equipment, etc. It can solve the problems of poor emulsification performance, high price, difficult emulsification, etc., and achieve low cost, good stability, and Excellent emulsifying performance

Active Publication Date: 2016-03-02
JIANGXI GANZHOU GUOTAI SPECIALTY CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the emulsifying performance is relatively poor, and it is difficult to emulsify. In addition, the raw material for its production is polyamine, and the price is relatively high

Method used

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  • A kind of emulsifier for emulsion explosive and preparation method thereof
  • A kind of emulsifier for emulsion explosive and preparation method thereof
  • A kind of emulsifier for emulsion explosive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Mix 80g of polyisobutylene succinic anhydride (Mn=1030g / mol) with a saponification value of 108.86mg / gKOH, 20g of hexaglycerol and 80g of n-octane. Under the protection of nitrogen, heat up to 80°C and stir for 4 hours. After the reaction , remove the solvent to obtain emulsifier P1 according to the present invention.

Embodiment 2

[0026] Mix 80 g of polyisobutylene succinic anhydride (Mn=1030 g / mol) with a saponification value of 108.86 mg / gKOH, 35 g of hexaglycerol and 100 g of n-octane, and add a catalyst whose mass (acid anhydride and polyglycerol total mass) fraction is 1.0%. For p-toluenesulfonic acid, under the protection of nitrogen, the temperature was raised to 120°C, and the reaction was stirred for 2.5 hours. After the reaction, the solvent was removed to obtain the emulsifier P2 of the present invention.

Embodiment 3

[0028] Mix 80g of polyisobutylene succinic anhydride (Mn=1030g / mol) with a saponification value of 108.86mg / gKOH, 70g of hexaglycerol and 120g of n-octane, and add a catalyst with a mass fraction of 1.5% (acid anhydride and polyglycerol total mass) For p-toluenesulfonic acid, under the protection of nitrogen, the temperature was raised to 130°C, and the reaction was stirred for 9.0 hours. After the reaction, the solvent and unreacted glycerin were removed to obtain the emulsifier P3 of the present invention.

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Abstract

The invention relates to an emulsifier for an emulsion explosive and a preparation method for the emulsifier. The emulsifier is a poly-alkyl carboxylic acid polyglycerol ester-type emulsifier obtained by performing esterification on poly-alkyl succinic anhydride and polyglycerol, wherein the component of the poly-alkyl succinic anhydride is 500-3500, and the degree of polymerization of the polyglycerol is 2-12. The emulsifier is good in emulsifying property. When the emulsion explosive is prepared, an emulsion can be easily formed, and the storage stability of the emulsion explosive is improved. The emulsifier is suitable for preparing the emulsion explosive with a longer storage time.

Description

technical field [0001] The invention relates to an emulsifier mainly used for preparing emulsion explosives and a preparation method thereof. Background technique [0002] Emulsifier is a key and important component used in the emulsion explosive industry. It makes the oxidant water phase and fuel oil phase form a water-in-oil emulsion explosive matrix and also has dispersion effects; the performance of the emulsifier determines the explosion of the emulsion explosive. performance and storage performance. [0003] At present, the emulsifiers used in the production of emulsion explosives are mainly SPAN-80 and polybutene butadiimine (single-hanging and double-hanging) emulsifiers. The advantage of SPAN-80 is that it is easy to emulsify, and it can form a latex matrix at a lower temperature and lower rotational speed, but the molecular structure contains double bonds, which are easy to demulsify and crystallize after being oxidized, making the emulsified emulsion prepared by ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C06B23/00
Inventor 许虎君罗强章宋春丽
Owner JIANGXI GANZHOU GUOTAI SPECIALTY CHEM
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