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Fast mixing reactor and application thereof

A technology of mixing reactors and reactors, applied in fluid mixers, mixers, chemical/physical/physical-chemical stationary reactors, etc., can solve the problems of poor reaction effect, uniform mixing, and increased side reactions, etc. Achieve the effect of fast mixing, fast mixing and fast response

Active Publication Date: 2013-09-04
WANHUA CHEM GRP CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the flow rate of the streams is relatively low, it is relatively easy to mix the two streams, but when the production capacity is large, due to the enlargement of the flow channel, the two streams cannot be mixed evenly in a short period of time. A mixing distance is bound to be required, so that the chances of side reactions are greatly increased
Since the production capacity of the above two mixers has the maximum limit, and the reaction effect under high load becomes worse, it is necessary to develop more effective rapid mixing equipment to achieve rapid mixing and rapid reaction between materials under large-scale production capacity

Method used

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  • Fast mixing reactor and application thereof
  • Fast mixing reactor and application thereof
  • Fast mixing reactor and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] use image 3 The rapid mixing reactor shown was used for production trials of MDI. Among them, the first feed distributor such as Figure 6c As shown, some diameters are evenly distributed on the first feed distributor as circular channels of 20mm, and the outlet velocity of the phosgene solution through the first feed distributor circular channels is 6m / s; The opening method of the second feed injection port is as follows: Figure 5c As shown, the diameter of the opening is 10mm, the outlet velocity of the amine solution through the second feed injection port is 16m / s; the rotational speed of the rotating shaft is 1200rpm. The reactor is tested on the MDI device, the test load is 220,000 tons of MDI / year, the feed rate of the amine solution is 24t / h, chlorobenzene is used as the reaction solvent, and the mass concentration of the chlorobenzene solution of the amine is 33%. The chlorobenzene solution of amine is sprayed into the reactor shell through the rotating hol...

Embodiment 2

[0065] use image 3 The rapid mixing reactor shown was used for production trials of MDI. Among them, the first feed distributor such as Figure 6b As shown, arc-shaped slits with different inner diameters are uniformly distributed on the first feed distributor, and the radial width of the slits is 2 mm; the exit velocity of the phosgene solution passing through the arc-shaped slits is 10 m / s. The opening method of the second feed injection port on the hollow impeller material distributor is as follows: Figure 5b As shown, the injection port is a rectangle of 3mm×8mm; the exit velocity of the amine solution through the second feed injection port is 22m / s. The rotational speed of the rotating shaft was 1400 rpm. The reactor is tested on the MDI device, the test load is 300,000 tons of MDI / year, the feed rate of the amine solution is 33t / h, chlorobenzene is used as the reaction solvent, and the mass concentration of the chlorobenzene solution of the amine is 33%. The chloro...

Embodiment 3

[0068] use Figure 4 The rapid mixing reactor shown was tested for the production of polymethylene polyphenyl polyamines. Among them, the first feed distributor such as Figure 6b As shown, arc-shaped slits with different inner diameters are evenly distributed on the first feed distributor, and the radial width of the slits is 6 mm; the outlet velocity of the mixed solution of aniline hydrochloride and circulating fluid through the arc-shaped slit is 5m / s. The opening method of the second feed injection port on the hollow impeller material distributor is as follows: Figure 5b As shown, the injection port is a rectangle of 3mm×8mm; the exit velocity of the formaldehyde solution through the second feed injection port is 20m / s. The rotational speed of the rotating shaft was 2400 rpm. Adopt this reactor to test on the device of polymethylene polyphenyl polyamine, test load is 300,000 tons of polyamine / year, formaldehyde solution (mass fraction 37%) feed rate is 16t / h, formald...

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Abstract

The invention discloses a fast mixing reactor and the application thereof. The fast mixing reactor comprises a first feeding passage casing, a reactor casing, a second feeding passage, a hollow impeller material dispenser, a rotating shaft and a first feeding dispenser, wherein the first feeding passage casing and the reactor casing are coaxially arranged and communicated with each other; the second feeding passage, the hollow impeller material dispenser and the rotating shaft are arranged along the central line of the fast mixing rector; the hollow impeller material dispenser is arranged inside the reactor casing and can rotate inside the reactor casing under the driving of the rotating shaft; the second feeding passage is communicated with the hollow impeller material dispenser; at least one first feeding port is formed on the first feeding passage casing; at least one reaction liquid outlet is formed at the tail end of the reactor casing; and feeding jet orifices are formed on the first feeding dispenser and the hollow impeller material dispenser. The fast mixing rector can realize instant quick mixing of two materials under the condition of relatively high production capability, so that the yield and the quality of target products can be improved.

Description

technical field [0001] The invention relates to a rapid mixing reactor, more specifically, a dynamic reactor capable of realizing rapid mixing and rapid reaction between fluids under large-scale production capacity. At the same time, the invention also provides a method for preparing isocyanate by phosgenation using the reactor, and a method for preparing polymethylene polyphenyl polyamine by aniline and formaldehyde using the reactor. Background technique [0002] In some chemical production processes, when complex fast parallel competitive reactions or fast serial competitive reactions occur between the reaction materials, the reaction products or intermediate products may further react with a certain component of the raw materials; the degree of these reactions is related to each There is a direct relationship between the concentration distribution of the material. Therefore, the initial mixing effect between materials will greatly affect the final product distribution, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J19/18B01J4/00B01F5/04C07C263/10C07C265/14
Inventor 丁建生孙德镇华卫琦侯庆乐王文波于学丽
Owner WANHUA CHEM GRP CO LTD
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