Conductive super-hydrophobic paint and production method thereof
A technology of super-hydrophobic coatings and production methods, applied in conductive coatings, epoxy resin coatings, coatings, etc., can solve problems such as commercial products not appearing in the market, and achieve good solubility, large aspect ratio, phase Capacitive effect
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Embodiment 1
[0033] Add 50g of xylene, 30g of n-hexane, and 120g of cyclohexanone mixed diluent to 50g of carbon nanotubes with a length of 20 microns and an aspect ratio greater than 150 times, disperse for 20 minutes with an ultrasonic disperser with a power of 20KHz, and disperse to form carbon nanotubes Predispersion.
[0034] Hydrophobic fumed silica modification process: 10 parts of commercially available fumed silica was ultrasonically dispersed in 90 parts of xylene for 30 minutes to make a 10% particle dispersion, and 12 parts of modifier (dodecafluoroheptyl Propyl siloxane) was added to 100 parts of the particle dispersion at a temperature of 45-65°C for 4 hours of modification reaction. After the reaction, the mixture was centrifuged and washed three times repeatedly. After centrifugation and vacuum drying, hydrophobic fumed silica was obtained.
[0035] Mix 120g of 50% cyclohexanone solution of epoxy E-44, 30g of hydrophobic fumed silica, 100g of xylene, 60g of n-hexane, and 2...
Embodiment 2
[0039] Add 50g of xylene, 30g of butyl acetate, and 240g of cyclohexanone mixed diluent to 80g of carbon nanotubes with a length of 10 microns and an aspect ratio greater than 150 times, and disperse for 20 minutes with an ultrasonic disperser with a power of 20KHz to form carbon nanotubes. tube of predispersion.
[0040] Hydrophobic fumed silica modification process: 10 parts of commercially available fumed silica was ultrasonically dispersed in 90 parts of xylene for 30 minutes to make a 10% particle dispersion, and 10 parts of modifier (dodecafluoroheptyl Propyl siloxane) was added to 100 parts of the particle dispersion at a temperature of 45-65°C for 4 hours of modification reaction. After the reaction, the mixture was centrifuged and washed three times repeatedly. After centrifugation and vacuum drying, hydrophobic fumed silica was obtained.
[0041] Mix 200g of 50% cyclohexanone solution of epoxy E-20, 20g of hydrophobic fumed silica, 30g of xylene, 15g of butyl acetat...
Embodiment 3
[0045] Add 80g of xylene, 40g of ethyl acetate, and 280g of cyclohexanone mixed diluent to 90g of carbon nanotubes with a length of 5 microns and an aspect ratio greater than 150 times, and disperse for 40 minutes with an ultrasonic disperser with a power of 20KHz to form carbon nanotubes. tube of predispersion.
[0046] Hydrophobic fumed silica modification process: 10 parts of commercially available fumed silica was dispersed ultrasonically in 90 parts of xylene for 30 minutes to make a 10% particle dispersion, and 8 parts of modifier (dodecafluoroheptyl Propyl siloxane) was added to 100 parts of the particle dispersion at a temperature of 45-65°C for 4 hours of modification reaction. After the reaction, the mixture was centrifuged and washed three times repeatedly. After centrifugation and vacuum drying, hydrophobic fumed silica was obtained.
[0047] Mix 240g of 50% cyclohexanone solution of epoxy E-20, 10g of hydrophobic fumed silica, 20g of xylene, 10g of n-hexane, and ...
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