Method for preparing compound controlled-release fertilizer from pulverized fuel ash serving as raw material
A fly ash and composite technology, applied in the direction of fertilizer mixture, fertilization device, application, etc., can solve the problems of water body and environmental pollution, low fertilizer utilization rate, low fertilizer utilization rate, etc., to prevent the loss of nitrogen fertilizer and good social benefits And economic benefits, the effect of low production cost
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Embodiment 1
[0019] Preparation of compound loss-controlling fertilizer using fly ash as raw material:
[0020] a) 5.0g of fly ash is placed in a muffle furnace for roasting, the roasting temperature is 600°C, and the roasting time is 2 hours; the roasted fly ash is acid-dissolved for 2 hours with 15ml of 2mol / L hydrochloric acid , the temperature is maintained at 80°C to obtain pretreated fly ash;
[0021] b) The pretreated fly ash, industrial aluminum hydroxide, sodium carbonate, and polyaluminum ferric chloride are mixed in a mass ratio of 7:1:8:7; the ingredients are roasted in a muffle furnace for 1 hour , the roasting temperature is 1000°C to obtain the roasted product;
[0022] c) Under stirring conditions, put all the roasted products into deionized water, raise the temperature to 40°C, keep the temperature at a constant temperature for 2 hours, and take the liquid to make up alkali until neutral;
[0023] d) heating the mixed solution to 100°C, and crystallizing for 3 hours unde...
Embodiment 2
[0026] Preparation of compound loss-controlling fertilizer using fly ash as raw material:
[0027] a) 5.0g fly ash is placed in a muffle furnace for roasting, the roasting temperature is 1000°C, and the roasting time is 4 hours; the roasted fly ash is acid-dissolved for 3 hours with 15ml 2mol / L sulfuric acid, The temperature is maintained at 60°C to obtain pretreated fly ash;
[0028] b) The pretreated fly ash, industrial aluminum hydroxide, sodium carbonate, and polyaluminum ferric chloride are mixed with a mass ratio of 10: 1.5: 15: 10; the ingredients are placed in a muffle furnace and roasted for 1 hour, The calcination temperature is 1000°C to obtain a calcination product;
[0029] c) Under the condition of stirring, all the roasted products are immersed in deionized water, warmed to 50°C, kept at a constant temperature for 2 hours, and the liquid is taken to make up alkali until neutral;
[0030] d) heating the mixed solution to 100°C, and crystallizing for 7 hours und...
Embodiment 3
[0033] Preparation of compound loss-controlling fertilizer using fly ash as raw material:
[0034] a) The fly ash of 5.0g is placed in the muffle furnace and roasted, the roasting temperature is 1000 ℃, and the roasting time is 3 hours; add the sulfuric acid of 7.5ml 2mol / L and the hydrochloric acid of 7.5ml 2mol / L to the roasted The fly ash was acid-dissolved for 3 hours, and the temperature was kept at 90°C to obtain pretreated fly ash;
[0035] b) Pretreatment fly ash, industrial aluminum hydroxide, sodium carbonate, and polyaluminum ferric chloride are mixed at a mass ratio of 20:0.5:3:15; the ingredients are roasted in a muffle furnace for 1 hour, and the roasting The temperature is 1000°C to obtain a roasted product;
[0036] c) Under stirring conditions, immerse all the roasted products in deionized water, raise the temperature to 50°C, keep the temperature at a constant temperature for 2 hours, and take the liquid to make up alkali until neutral;
[0037] d) heating ...
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