Catalyst for hydro-conversion of mixed aqueous solution containing alcohol, aldehyde, acid and ester into alcohols
A technology for hydroconversion and catalyst, used in the preparation of organic compounds, organic chemistry, bulk chemical production, etc.
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Embodiment 1
[0023] The catalyzer of embodiment 1 is 5%Re-2%Ag-1.5%Pd / coconut shell activated carbon (the activated carbon is not pretreated before use). Weigh 100 grams of commercial coconut shell charcoal (20-40 mesh), and dry at 120° C. for 10 hours. Configuration 105ml contains 7.872 grams of NH 4 ReO 4 , 3.442 g AgNO 3 and 3.550 g Pd(NO 3 ) 2 Aqueous solution, use this aqueous solution to impregnate the above-mentioned coconut shell activated carbon carrier, dry naturally, dry in 120 ℃ of oven nitrogen atmospheres for 4 hours, roast in 300 ℃ of nitrogen atmospheres for 5 hours. Before the reaction, in hydrogen at 250°C (0.2Mpa, 2500h -1 ) reduction activation for 4 hours.
Embodiment 2
[0025] Catalyst 5%Re-2%Ag-1.5%Pd / coconut shell activated carbon of embodiment 2 (pretreatment before activated carbon is used). Weigh 100 grams of commercial coconut shell charcoal (20-40 mesh), wash with deionized water until the conductivity is about 15, and dry at 120° C. for 10 hours. Other steps are the same as in Example 1.
Embodiment 3
[0027] Catalyst 5%Re-2%Ag-1.5%Pd / almond core activated carbon of embodiment 3 (without pretreatment before activated carbon). Take by weighing 100 grams of commercial almond charcoal (20-40 orders). Dry at 120°C for 10 hours. Other steps are the same as in Example 1.
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