Vitamin E and organic germanium composite core-containing microcapsule finishing agent and preparation and application thereof
A technology of microcapsule finishing and organic germanium, which is applied in the direction of microcapsule preparation, microsphere preparation, fiber treatment, etc., can solve the problems of dry skin, rough skin, excessive aging, etc., and achieve anti-aging, high added value, and high-efficiency anti-oxidation Effect
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Embodiment 1
[0029] The salad oil, vitamin E and organic germanium were weighed respectively and stirred evenly under a magnetic stirrer to obtain a compound oil; the organic germanium content in the compound oil was 0.01%, and the vitamin content was E5%.
[0030] Weigh 10 grams of compound oil and add it into a three-necked bottle, add 2.1% of the weight of the compound oil Span 60 and 2.9% of Tween 60, heat up to 30-50 degrees under stirring conditions, and add 0-3% anion high 85 grams of aqueous solution of molecular emulsion stabilizer CMC is added dropwise to the oil phase at a certain speed, and the compound oil is emulsified in water under magnetic stirring, and the mechanical emulsification time is 2-4 hours.
[0031] Weigh 37 grams of melamine-formaldehyde prepolymer (80% solid content) and add it to the above emulsion, add 5% citric acid dropwise at a rate of 0.5mL / min to adjust the pH to 3.5-4, heat to 60°C, and keep warm for 1h. Then the temperature was raised to 90°C, and the...
Embodiment 2
[0033] The olive oil, vitamin E and organic germanium were weighed and stirred evenly under a magnetic stirrer to obtain a compound oil; the content of organic germanium in the compound oil was 0.8%, and the content of vitamin E was 10%.
[0034] Weigh 10 grams of compound oil and add it into a three-necked bottle, add 2.1% of the weight of the compound oil Span 60 and 2.9% of Tween 60, heat up to 30-50 degrees under stirring conditions, and add 0-3% anion high 85 grams of aqueous solution of molecular emulsion stabilizer CMS is added dropwise to the oil phase at a certain speed, and the compound oil is emulsified in water under magnetic stirring, and the mechanical emulsification time is 2-4 hours.
[0035] Weigh 19 grams of melamine-formaldehyde prepolymer (80% solid content) and add it to the above emulsion, add 5% citric acid dropwise at a rate of 0.5mL / min to adjust the pH value to 3.5-4, heat to 60°C, and keep warm for 0.5h , and then the temperature was raised to 90°C, ...
Embodiment 3
[0037] Cotton fabric vitamin E / organic germanium composite microcapsule finishing process:
[0038] Process prescription: 30g of microcapsule finishing in Example 1
[0039] Low temperature adhesive (40%) 45g
[0040] water x
[0041] Total: 1000g
[0042] Process flow:
[0043] Cotton fabric--padding (rolling liquid rate 130%)--hot air drying--baking at 120 degrees for 3 (min)--finished product.
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