Multifunctional textile finishing agent, preparation method thereof and cotton textile finishing method
A fabric finishing agent and multi-functional technology, applied in the direction of textiles and papermaking, fiber treatment, plant fiber, etc., can solve the problems of poor fixation effect, insufficient anti-wrinkle durability, etc., and achieve convenient processing, good anti-wrinkle effect and simple process Effect
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Embodiment example 1
[0040] The preparation steps of ecological multifunctional fabric finishing agent are as follows:
[0041] (1) Boil silk into 0.5% Na by weight 2 CO 3 Degumming in the solution for 3 times, 30 minutes each time, rinsing with hot water for 3 times, then drying at 55°C and cutting into pieces, the amount of silk used is 0.5% Na 2 CO 3 1.5% of the solution.
[0042] (2) According to the molar ratio, anhydrous calcium chloride: ethanol: water = 1:2:8 to make a ternary solution, and dissolve the silk fiber obtained in step (1) in the above ternary solution at 75°C After 180 minutes, filter the fibroin solution, put it into a dialysis bag, place it in clean water for dialysis, change the water every 2 hours, and concentrate it after 3 days of dialysis to obtain a silk fibroin solution. The amount of the above ternary solution is 15 times the dosage.
[0043] (3) Add 3.0mol / L hydrochloric acid solution to the silk fibroin solution in step (2), hydrolyze at 60°C for 150 minutes, ...
Embodiment example 2
[0047] The preparation steps of ecological multifunctional fabric finishing agent are as follows:
[0048] (1) Boil silk into 0.5% Na by weight 2 CO 3 Degumming in the solution 3 times, 30 minutes each time, rinsing 3 times with hot water, then drying and cutting at 65 °C, the amount of silk is 0.5% Na 2 CO 3 3% of the solution.
[0049](2) According to the molar ratio, anhydrous calcium chloride: ethanol: water = 1:2:8 to make a ternary solution, and dissolve the silk fiber obtained in step (1) in the above ternary solution at 75°C After 120 minutes, filter the silk fibroin solution, put it into a dialysis bag, place it in clean water for dialysis, change the water every 3 hours, and get the silk fibroin solution after 3 days of dialysis. The amount of the above ternary solution is the amount of silk 20 times.
[0050] (3) Add 3.0mol / L hydrochloric acid solution to the silk fibroin solution in step (2), hydrolyze at 70°C for 120 minutes, titrate to neutral with 3mol / L so...
Embodiment example 3
[0054] The steps of finishing the cotton fabric with the ecological multifunctional fabric finishing agent containing silk fibroin and chitosan are as follows:
[0055] (1) plain weave cotton fabric (150g / m 2 ) soaked in a sodium hydroxide solution with a concentration of 21% by mass, soaked at room temperature for 30 minutes, took it out, washed with water until neutral, and wrung out to obtain an alkali-treated cotton fabric. The consumption of sodium hydroxide solution is 40 times of cotton fabric weight.
[0056] (2) The alkali-treated cotton fabric obtained in step (1) was dipped twice and rolled twice in the ecological multifunctional fabric finishing agent of Example 1. The ecological multi-functional fabric finishing agent is 30 times the weight of cotton fabric, the soaking time is 40 minutes, and the squeeze rate is 85%.
[0057] (3) The cotton fabric obtained by padding in step (2) was pre-baked at 80°C for 60 minutes, and then baked at 130°C for 3 minutes to comp...
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