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High temperature nylon PPA reinforcing material and preparation method thereof

A reinforcing material, nylon technology, applied in the field of high-temperature nylon PPA reinforced material and its preparation, can solve the problems of difficult processing and poor fluidity, and achieve the effects of simplified processing, broad application prospects, and reduced processing temperature

Active Publication Date: 2010-09-01
徐东
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to its high temperature resistance, its fluidity is poor, which makes processing more difficult. Special process parameters must be used so that machinery and equipment can produce well

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Take by weight 40 parts of polyphthalamide (PPA), 20 parts of polyamide (PA66), 10 parts of main flame retardant PBS-64HW, 4 parts of auxiliary flame retardant Sb2O3, 40 parts of long glass fiber 988A , antioxidants 1010 and 168 are 0.3 parts, lubricants TAF and siloxane are 0.3 parts, and nucleating agent CAV102 is 0.3 parts.

[0035] Composite materials were prepared by the following methods:

[0036]a. Weighing the raw materials and drying them respectively, including drying polyphthalamide (110°C for 3h) and polyamide (90°C for 4h);

[0037] b. Add the dried polyphthalamide and polyamide into the high-speed mixer, and add lubricant, nucleating agent and antioxidant, and mix at high speed for about 4 minutes;

[0038] c. Put the main flame retardant and auxiliary flame retardant into the high-speed mixer and mix for about 8 minutes. After mixing, add the mixed flame retardant to the previously mixed material and mix for about 6 minutes. Put the good material into t...

Embodiment 2

[0042] Weigh 35 parts of polyphthalamide (PPA), 10 parts of polyamide (PA66), 11.5 parts of main flame retardant PBS-64HW, 3.5 parts of auxiliary flame retardant Sb2O3, 40 parts of long glass fiber 988A by weight , antioxidants 1010 and 168 are 0.3 parts, lubricants TAF and siloxane are 0.3 parts, and nucleating agent CAV102 is 0.3 parts.

[0043] Composite materials were prepared by the following methods:

[0044] a. Weighing the raw materials, and drying the raw materials respectively, including drying polyphthalamide (120°C 3h) and polyamide (95°C 4h);

[0045] b. Add the dried polyphthalamide and polyamide into the high-speed mixer, and add lubricant, nucleating agent and antioxidant, and mix at high speed for about 4 minutes;

[0046] c. Put the main flame retardant and auxiliary flame retardant into the high-speed mixer and mix for about 7 minutes. After mixing, add the mixed flame retardant to the previously mixed material and mix for about 8 minutes. Put the good mat...

Embodiment 3

[0051] Weigh 34 parts of polyphthalamide (PPA), 9.5 parts of polyamide (PA66), 11.5 parts of main flame retardant PBS-64HW, 3.5 parts of auxiliary flame retardant Sb2O3, 40 parts of long glass fiber T635B , antioxidants 1010 and 168 are 0.3 parts, lubricants TAF and siloxane are 0.3 parts, and nucleating agent CAV102 is 0.3 parts.

[0052] Composite materials were prepared by the following methods:

[0053] a. Weighing the raw materials, and drying the raw materials respectively, including drying polyphthalamide (130°C 3h) and polyamide (100°C 4h);

[0054] b. Add the dried polyphthalamide and polyamide into the high-speed mixer, and add lubricant, nucleating agent and antioxidant, and mix at high speed for about 5 minutes;

[0055] c. Put the main flame retardant and auxiliary flame retardant into the high-speed mixer and mix for about 9 minutes. After mixing, add the mixed flame retardant to the previously mixed material and mix for about 5 minutes. Put the good material i...

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PUM

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Abstract

The invention discloses a high temperature nylon PPA reinforcing material and a preparation method thereof. The high temperature nylon PPA reinforcing material comprises the following components in part by weight: 30 to 50 parts of polyphthalamide, 8 to 20 parts of polyamide, 10 to 15 parts of main fire retardant, 3 to 5 parts of assistant fire retardant, 30 to 45 parts of filling reinforcing agent, 0.2 to 0.6 part of antioxidant, 0.2 to 0.8 part of lubricant, and 0.3 to 0.6 part of nucleating agent. The invention overcomes the defects of lower liquidity and difficult processing of the PPA because a polyamide material is introduced; the polyamide material has the characteristics of high liquidity and similar molecular structure, and can be well fused with the PPA material, so that the liquidity is improved, the processing temperature is greatly reduced, and the processing procedure is simplified; and a modified material with excellent performance after being reinforced by a glass fiber is equal to foreign brand materials, and plays a role in laying the foundation for domestic volume production and future quantity demand in the domestic market.

Description

[technical field] [0001] The invention relates to the technical field of polymer materials, in particular to a high-temperature nylon PPA reinforcing material and a preparation method thereof. [Background technique] [0002] Polyphthalamide (referred to as PPA) is a new type of high-temperature-resistant, high-performance special engineering plastic that was first developed and mass-produced by Solvay. It has the advantages of high rigidity, high heat resistance, high strength and excellent electrical properties. Polyphthalamide is a semi-crystalline thermoplastic aromatic polyamide, commonly known as aromatic high-temperature nylon. It is a high-temperature-resistant material with a melting point of 310-325°C and a heat distortion temperature of 260°C. Between -280°C, its melting point is higher than that of PA46 and PPS; under high temperature and high humidity, the tensile strength of PPA is 20% higher than that of nylon 6, and higher than that of nylon 66; the flexural ...

Claims

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Application Information

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IPC IPC(8): C08L77/06C08L25/18C08K13/04C08K7/14B29B9/06
Inventor 徐东徐永郭宇嘉
Owner 徐东
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