MCrAlY+AlSiY composite coating and preparation technique thereof
A composite coating and preparation process technology, applied in the direction of metal material coating process, coating, layered products, etc., can solve the problems of increased brittleness of coating, decreased melting point, and unfavorable alternating cycle of cold and heat of coated parts, etc. Achieve the effect of improving high temperature oxidation resistance, prolonging service life and long service life
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Embodiment 1
[0023] The base material is Ni-based superalloy K465, and its nominal composition is (mass percentage): 9.75% Co, 8.75% Cr, 5.5% Al, 2.15% Ti, 1.85% Mo, 10.25% W, 1% Nb, Ni balance, Sample size is Φ15×1.5mm 2 . The MCrAlY+AlSiY composite coating was co-deposited by domestic MIP-8-800 multi-arc ion plating equipment. The composition of the MCrAlY target is as follows (by mass percentage), Co: 32; Cr: 20; Al: 8; Y: 0.5; Si: 1; B: 0.03, Ni: the balance. The sample is pretreated before deposition, that is, the substrate sample is polished to Ra=0.4 μm, wet sandblasting with 200-mesh hollow glass pellets, and then ultrasonically cleaned with metal detergent, deionized water, and acetone for 15 minutes, and washed with alcohol Rinse and tumble dry for later use. MIP-8-800 arc ion plating equipment was used to deposit conventional MCrAlY coatings, pre-evacuated to 7×10 -3 Pa, Ar gas was introduced during bombardment and deposition, and the vacuum degree was 2×10 -1 Pa. When cle...
Embodiment 2
[0028] The difference from Example 1 is:
[0029] The base material is directionally solidified Ni-based superalloy DZ125, and its nominal composition is (in terms of mass percentage): 10% Co, 9% Cr, 7% W, 5% Al, 2.5% Ti, 3.5% Ta, trace amount of C, Ni quantity. Sample size is 15×10×1.5mm 3 . Coating deposition parameters are the same as in Example 1. The MCrAlY+AlSiY composite coating was put into a quartz glass tube to be evacuated and then filled with Ar gas for protection. It was kept in a muffle furnace at 1000 °C for 5 h with a heating rate of 6 °C / min, and then cooled to room temperature with the furnace.
[0030] The cross-sectional morphology of the coating before and after diffusion annealing is as follows: image 3 shown by image 3 It can be seen that after diffusion annealing, the thickness of the surface layer of MCrAlY+AlSiY composite coating is about 15 μm, composed of β-NiAl and σ-NiCoCr, the content of Al is about 20wt%, the content of Cr is about 10wt%,...
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