Extraction process of clerodendranthus spicatus
An extraction process, kidney tea technology, applied in medical preparations containing active ingredients, plant raw materials, blood diseases, etc., can solve the problem of loss of beneficial ingredients of kidney tea, and achieve enhanced anti-inflammatory effects
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Embodiment 1
[0016] 1. Cleaning and drying process: take the kidney tea raw material, remove the sundries, wash with water, and dry in the sun.
[0017] 2. Crushing process: crush the sun-dried kidney tea into 40-80 mesh particles.
[0018] 3. Pretreatment process: add water and cellulosic mold to the crushed kidney tea granules, react at 30-35°C for 5 hours, then raise the temperature to 50-60°C, react for 2 hours, cool to room temperature, filter, that is Yes; the weight ratio of kidney tea and water is 1:4, and the weight / volume (kg / L) ratio of kidney tea and compound cellulase is 1:0.02.
[0019] The compound cellulosic mold is a mixture of Trichoderma sp CGMCC 3.3068 and Trichoderma koningii CGMCC 3.2774, and the volume ratio of the expansion medium is 1:0.5.
[0020] 4. The post-treatment process is: extract the filtrate with ether three times, combine the ether extracts, and evaporate to dryness at 50°C to obtain a tan extract. The volume ratio of the filtrate to ether is 1:0.5. T...
Embodiment 2
[0022] 1. Cleaning and drying process: take the kidney tea raw material, remove the sundries, wash with water, and dry in the sun.
[0023] 2. Crushing process: crush the sun-dried kidney tea into 100-200 mesh particles.
[0024] 3. Pretreatment process: add water and cellulosic mold to the crushed kidney tea granules, react at 35-40°C for 2 hours, then raise the temperature to 50-60°C, react for 2 hours, cool to room temperature, filter, that is Yes; the weight ratio of kidney tea and water is 1:10, and the weight / volume (kg / L) ratio of kidney tea and compound cellulase is 1:0.1.
[0025] The compound cellulosic mold is a mixture of Trichoderma sp CGMCC 3.3068 and Trichoderma koningii CGMCC 3.2774, and the volume ratio of the expansion medium is 1:0.8.
[0026] 4. The post-treatment process is: extract the filtrate with ether three times, combine the ether extracts, and evaporate to dryness at 50°C to obtain a tan extract. The volume ratio of the filtrate to ether is 1:0.5. ...
Embodiment 3
[0028] Except that the kidney tea extract that has been cooled to room temperature was ultrasonically extracted for 20 minutes in an ultrasonic wave with a frequency of 25,000 Hz, the rest was the same as in Example 1. The yield of extract is 14.5% based on kidney tea raw material.
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