Preparation process of resveratrol
A preparation process, the technology of resveratrol, applied in the field of drug preparation, can solve the problems of low conversion rate and long extraction time, and achieve the effect of increased conversion rate, improved extraction rate and thorough enzymatic hydrolysis
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Embodiment 1
[0044] Take 10kg knotweed raw material as an example, after the raw knotweed cuspidatum is rinsed to remove dust, cut into slices with a thickness of 2mm for use; put the ready-to-use material into the digestion tank, add 200kg enzymatic hydrolysis solution, and adjust the pH value to 0.1mol / L hydrochloric acid solution 4. Carry out enzymatic hydrolysis; the enzymatic hydrolysis solution is a 1% combined enzyme solution, which includes 1 kg distiller's yeast and 1 kg cellulase.
[0045] Extraction: ① Concentration and filtration: After 2 hours of enzymolysis, the raw material after enzymolysis is transferred to an extraction tank, extracted by 3 times the organic solution, and the extract is recovered and concentrated under reduced pressure and filtered; the organic solution is 75% ethanol solution. ②Extraction: Extract the recovered and concentrated liquid with purified water at a ratio of 1:1, repeat 4 times and recover the organic phase to obtain the crude product; ③Refinin...
Embodiment 2
[0047] Add the enzymolysis solution according to the ratio of 1:3 to the mass ratio of the materials to be used, the enzymolysis solution is a 0.6% combined enzyme solution, and the combined enzyme includes 1 part of distiller's yeast, 0.5 part of cellulase, 0.2 part of Lactic acid bacteria. All the other are the same as embodiment 1
Embodiment 3
[0049] Add the enzymolysis solution according to the ratio of 1:2 to the mass ratio of the materials to be used, the enzymolysis solution is a 1.5% combined enzyme solution, and the combined enzyme includes 1 part of distiller's yeast, 0.4 part of cellulase, 0.1 part of Lactic acid bacteria.
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