Electrolyte for the galvanic deposition of aluminium from aprotic solvents in a plating barrel
An electrolyte and aprotic technology, which is applied in the fields of compounds containing group 3/13 elements of the periodic table, chemical instruments and methods, organic chemistry, etc., can solve problems such as deficiencies, and achieve high plating ability and uniform corrosion resistance.
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[0054] 1. Electrolyte Preparation
[0055] Tetraethylammonium chloride, which is commercially available as the monohydrate, was dried under vacuum. 1 mol of dried tetraethylammonium chloride was mixed with toluene so as to obtain a suspension. 2 mol (used neat or as a solution in toluene) of triethylaluminum were added dropwise to the suspension during cooling. The reaction mixture was stirred. Get N(C 2 h 5 ) 4 Cl 2Al(C 2 h 5 ) 3 • 2 Clear solutions in toluene. 2 mol of toluene was used as a solvent relative to the amount of tetraethylammonium chloride used. The resulting product was used as an electrolyte.
[0056] 2. The conductivity of the electrolyte of the present invention is compared to the conductivity of the prior art electrolyte
[0057] Sufficient conductivity of the electrolyte is an essential requirement for adequate coating, especially of small parts in coating drums. The conductivity of the electrolytes of the present invention is significantly high...
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