Multifunctional in-situ electro-chemical measuring apparatus for tensile test
An in-situ electrochemistry and measurement device technology, applied in the field of electrochemistry, can solve problems such as differences, errors, and incomplete experimental data, and achieve the effects of complete data points, easy operation, and reliable experimental data.
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Embodiment 1
[0021] Example 1: Install the multifunctional in-situ electrochemical measuring device required for the tensile test to conduct the electrochemical test of the three-electrode system (simulation of a specific gas environment in the solution)
[0022] 1. Load the multifunctional in-situ electrochemical measuring device into the stretching machine, in which the chamber 13 falls on the lower chuck 15.
[0023] 2. Seal the tensile specimen 1 with the wire welded and the upper and lower chucks 14, 15 with 704 silica gel, leaving an area of the predetermined value for the test.
[0024] 3. Install the salt bridge 2, the thermocouple 4, and the rubber plug 10 into the top cover 12, and insert the metal platinum auxiliary electrode 3 into the rubber plug 10.
[0025] 4. Put the rubber plug 10 into the cavity 13, and pass the tensile sample 1 through the rubber plug in the cavity 13 and the top cover 12. The rotating top cover 12 and the chamber 13 are closed,
[0026] 5. Install the hea...
Embodiment 2
[0030] Example 2: Install the multifunctional in-situ electrochemical measuring device required for the tensile test to conduct the electrochemical test of the three-electrode system (simulation of the alternate dry and wet environment)
[0031] 1. Load the multifunctional in-situ electrochemical measuring device into the stretching machine, in which the chamber 13 falls on the lower chuck 15.
[0032] 2. Seal the tensile specimen 1 with the wire welded and the upper and lower chucks 14, 15 with 704 silica gel, leaving an area of the predetermined value for the test.
[0033] 3. Install the salt bridge 2, the thermocouple 4, and the rubber plug 10 into the top cover 12, and insert the metal platinum auxiliary electrode 3 into the rubber plug 10.
[0034] 4. Put the rubber plug 10 into the cavity 13, and pass the tensile sample 1 through the rubber plug in the cavity 13 and the top cover 12. The rotating top cover 12 and the chamber 13 are closed,
[0035] 5. Close the air inlet ...
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