Microwave extraction method for purple cabbage haematochrome
An extraction method and technology for purple cabbage, which are applied to chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problems of reports, and there is no microwave extraction method for purple cabbage pigment, and achieve simple steps and high anthocyanin content. , the effect of easy operation
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Embodiment 1
[0007] Weigh 10g of fresh purple cabbage and cut them into 0.2cm×0.2cm pieces, add 0.35mol / L hydrochloric acid 100ml and soak for 30 minutes, put them in a microwave oven, control the microwave power at 900W, heat for 120 seconds, take it out and cool and filter Repeat the operation twice. After the extract is concentrated under reduced pressure, it is purified by macroporous resin, washed with water and eluted with 30% ethanol, and the eluate is concentrated and dried under reduced pressure to obtain the purple cabbage pigment product.
Embodiment 2
[0009] Weigh 10g of dried purple cabbage, crush it, pass through a 60-mesh sieve, add 0.35mol / L hydrochloric acid 200ml and soak for 30 minutes, put it in a microwave oven, control the microwave power at 900W, heat for 120 seconds, take it out and cool and filter, repeat the operation twice Next, the extract is concentrated under reduced pressure, purified by a macroporous resin, washed with water and eluted with 50% ethanol, and the eluate is concentrated and dried under reduced pressure to obtain the purple cabbage pigment product.
Embodiment 3
[0011] Weigh 10 kg of fresh purple cabbage, crush it with a crusher, add 0.35mol / L hydrochloric acid 150L and soak for 60 minutes, put it in a microwave oven, control the microwave power at 900W, heat for 150 seconds, take it out and filter, and concentrate the extract under reduced pressure. Then, it is purified by macroporous resin, washed with water and eluted with 30% ethanol, and the eluate is concentrated and dried under reduced pressure to obtain the purple cabbage pigment product.
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