AI-based alloy sputtering target and process for producing the same
A technology of base alloy and sputtering target, which is applied in the field of Al-base alloy sputtering target and its preparation, can solve the problems of no proposal, high production cost, troublesome preparation method and the like
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[0038] 3. The method for preparing an Al-based alloy sputtering target according to item 1 or 2, the method comprising:
[0039] preparing a dense body of Al-based alloy; then
[0040] forging the dense body of the Al-based alloy to obtain a slab; then
[0041] rolling the slab at a rolling temperature of 400 to 500°C, a reduction ratio of 5 to 15% per pass, and a total reduction ratio of 60 to 90%; and then
[0042] Heating is performed at a temperature in the range of 300 to 400°C for 1 to 2 hours.
[0043] 4. The method according to item 3, wherein said preparation of the dense body of the Al-based alloy comprises:
[0044] Al-based alloy preforms are prepared according to the spray forming method, and
[0045]Al-based alloy preforms are densified by means of densification.
[0046] According to the Al-based alloy sputtering target of the present invention, since the crystallographic orientation in the normal direction of the sputtering surface is appropriately controll...
Embodiment 1
[0127] From Al-based alloys whose compositions are shown in Tables 1 and 2, Al-based alloy preforms (density: substantially 50 to 60%) were obtained according to the following spray forming method.
[0128] (Injection molding conditions)
[0129] Melt temperature: 1000°C
[0130] Gas / Metal Ratio: 6Nm 3 / kg
[0131] Spray distance: 1050mm
[0132] Gas atomizer outlet angle: 7°
[0133] Collector Angle: 35°
[0134] Subsequently, each preform obtained was sealed in a capsule, followed by degassing, and then densified with a HIP apparatus. The HIP treatment was performed at a HIP temperature of 550° C. for a HIP time of 2 hours at a HIP pressure of 85 MPa.
[0135] The Al-based alloy dense body thus obtained was forged under conditions of a heating temperature of 500° C. before forging, a heating time of 2 hours, and an upsetting ratio of 10% or less each time, thereby obtaining a slab (dimensions: thickness 60 mm, width 540mm and length 540mm).
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