Medicine for treating woman's dysmenorrhea and preparing process thereof
A medicine and a technology for dysmenorrhea, applied in the field of medicines for treating women's dysmenorrhea and their preparation, can solve the problems of failing to give full play to the multi-target comprehensive effects and single effects of traditional Chinese medicine compounds, and achieve the effects of no toxic side effects and reduced dosage.
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Embodiment 1
[0019] The medicinal ingredients are made of the following raw materials (percentage by weight): 70% of angelica, 20% of corydalis and 10% of cinnamon.
[0020] preparation:
[0021] 1. Crush the medicinal materials of Angelica sinensis through a 40-mesh sieve, soak in water for 4 hours, and steam distill for 4 hours to obtain Angelica sinensis oil for later use;
[0022] 2. Crush the cinnamon medicinal material through a 40-mesh sieve, place it in a supercritical CO2 extractor, extract at 40°C and 20MPa for 2 hours, and obtain cinnamon oil for later use;
[0023] 3. Crush the medicinal material of Corydalis Corydalis through a 40-mesh sieve, heat and extract with 70% ethanol at 50°C for 3 hours under reflux, filter with suction, evaporate the solvent, dissolve with sulfuric acid solution with a pH value of 3-4, filter, and pass the filtrate through cation exchange resin column. The cation exchange resin was basified with ammonia water, rinsed with 70% ethanol, and the eluat...
Embodiment 2
[0027] The medicinal ingredients are made of the following raw materials (percentage by weight): 43% of angelica, 43% of corydalis and 14% of cinnamon.
[0028] preparation:
[0029] 1. Crush the medicinal materials of Angelica sinensis through a 40-mesh sieve, soak in water for 4 hours, and steam distill for 4 hours to obtain Angelica sinensis oil for later use;
[0030] 2. Crush the cinnamon medicinal material through a 40-mesh sieve, soak in water for 4 hours, and steam distillation for 4 hours to obtain cinnamon oil for later use;
[0031] 3. Crush the medicinal material of Corydalis Corydalis through a 40-mesh sieve, soak in sulfuric acid solution with a pH value of 3-4 for 12 hours, filter, adjust the pH value of the filtrate to neutral with ammonia water, and add it to the macropore treated according to the instructions. On the adsorption resin column, first use about 3 times the amount of deionized water to elute, then use 5 times the amount of 50% ethanol to elute, c...
Embodiment 3
[0035] The medicinal ingredients are made of the following raw materials (percentage by weight): 16% of Angelica sinensis, 66% of Corydalis Corydalis, and 18% of cinnamon.
[0036] preparation:
[0037] 1. Crush the medicinal materials of Angelica sinensis through a 40-mesh sieve, place in a supercritical CO2 extractor, extract at 40°C and 25MPa for 3 hours, and obtain Angelica sinensis oil for later use;
[0038] 2. Crush the cinnamon medicinal material through a 40-mesh sieve, place it in a supercritical CO2 extractor, extract at 40°C and 20MPa for 2 hours, and obtain cinnamon oil for later use;
[0039] 3. Crush the medicinal material of Corydalis Corydalis through a 40-mesh sieve, extract with 70% ethanol at 50°C for 3 hours under reflux, filter with suction, evaporate the solvent, dissolve with sulfuric acid solution with a pH value of 3-4, filter, and pass the filtrate through a cation exchange resin column. Alkalinize the cation exchange resin with ammonia water, rins...
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