Carbon nanotube composite structure and method of manufacturing the same
a carbon nanotube and composite structure technology, applied in the field of carbon nanotube structure, can solve the problems of insufficient utilization of mechanical strength of carbon nanotube intrinsically, inability to obtain intended characteristics, and inability to achieve the desired characteristics, etc., to achieve the effect of reducing the length of the cross-linked site between the carbon nanotubes and stable chemical structur
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[0179] [Carbon Nanotube Composite Structure Using Glycerin-Cross-Linked Multi-Wall Carbon Nanotube Structure and Single-wall Carbon Nanotube Structure]
[0180] (First Addition Step)
[0181] 30 mg of multi-layer carbon nanotube powder (purity: 90%, average diameter: 30 nm, average length: 3 μm, available from Science Laboratory Inc.) was added to 20 ml of concentrated nitric acid (a 60 mass % aqueous solution, available from KANTO KAGAKU) for reflux at 120?C for 20 hours to synthesize a carbon nanotube carboxylic acid. A reaction scheme of the above is shown in FIG. 3. In FIG. 3, a carbon nanotube (CNT) portion is represented by two parallel lines (same applies for other figures relating to reaction schemes).
[0182] The temperature of the solution was returned to room temperature, and the solution was centrifuged at 5,000 rpm for 15 minutes to separate a supernatant liquid from a precipitate. The recovered precipitate was dispersed in 10 ml of pure water, and the dispersion liquid was s...
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