Ultraviolet light solidifying coating and preparation method thereof
A technology of curing coatings and ultraviolet light, applied in the direction of coatings, etc., can solve the problems of poor comprehensive performance of wear resistance and flexibility, and achieve the effect of good wear resistance and flexibility
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preparation example Construction
[0023]According to the preparation method of the UV-curable coating provided by the present invention, the mixing of the main resin, diluent, photoinitiator, hydroxyacrylate and isocyanate can be carried out simultaneously or step by step, preferably, the photoinitiator and Part of the diluent is mixed to fully dissolve the photoinitiator to obtain a solution containing the photoinitiator; uniformly mix the main resin with part of the diluent to obtain a slurry containing the main resin; uniformly mix the hydroxy acrylate with part of the diluent to obtain a solution containing Hydroxyacrylate slurry; mix the isocyanate curing agent and part of the diluent evenly to obtain a slurry containing isocyanate curing agent; then cure the solution containing photoinitiator, the slurry containing the main resin, the slurry containing hydroxyacrylate, and the isocyanate The slurry of diluent is mixed well, and finally the remaining diluent is added and mixed well.
[0024] The mixing te...
Embodiment approach
[0026] According to a preferred embodiment of the method provided by the present invention, the preparation method includes (1) uniformly mixing the photoinitiator with part of the diluent; (2) uniformly mixing the main resin with part of the diluent; (3) mixing the hydroxy acrylate Mix uniformly with part of the diluent; (4) mix the isocyanate with part of the diluent; (5) mix the products obtained in steps (1), (2), (3) and (4); (6) continue to add or Do not add leveling agent, defoamer, dispersant, and mix evenly; (7) cool down, filter the obtained slurry; (8) continue to add the remaining diluent, mix evenly.
[0027] In the method provided by the invention, the amount of each substance should be such that in the paint, the content of the main resin is 20-80% by weight, preferably 40-70% by weight, based on the total weight of the paint; The content is 5-60% by weight, preferably 10-50% by weight; the content of photoinitiator is 1-15% by weight, preferably 2-8% by weight;...
Embodiment 1
[0032] This example illustrates the coating provided by the invention and its preparation method.
[0033] Prepare the coating as follows: (1) mix 3 grams of photoinitiator Irgacure184 with 2 grams of diluent and stir until fully dissolved; Resin) and 20 trifunctional aliphatic urethane acrylate resins (Eternal products, 6136B-90 resins) are mixed with 10 grams of diluent at 40 ° C, and stirred evenly, (3) 25 grams of hydroxyl acrylic resins (Nuplex products, 4702 resins) ) mixed with 5 grams of diluent, stirred until fully dissolved; (4) 7 grams of isocyanate curing agent (Bayer product, model N3390) was mixed with 5 grams of diluent, stirred until fully dissolved; (5) step (1), The products obtained in (2), (3) and (4) are mixed; (6) the temperature is lowered, and the obtained slurry is filtered to remove residues to obtain coating T1. Wherein, the diluent used is a mixture of acetone, butyl acetate and xylene in a weight ratio of 2:1:1.
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