Preparation of air purifier for visible light responded titanium dioxide photocatalytic chamber
A technology of titanium dioxide and indoor air, which is applied in the field of preparation of indoor air purifier visible light-responsive titanium dioxide photocatalyst, which can solve the problems of weak and weak air purification effect
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Embodiment 1
[0015] a. First prepare a kinetically stable titanium dioxide ultrafine particle aqueous solution:
[0016] Slowly add 3.5 grams of hydrolyzable titanium-containing compound titanium tetrachloride into 200ml of deionized water at 1°C, and under the action of ultrasonic waves, the hydrolyzable titanium-containing compound is hydrolyzed and dispersed into a particle size of 10 nanometers -9 For rice-level ultrafine particles, the aqueous solution of ultrafine particles is clarified and transparent under visible light for use;
[0017] b. Add the rare metal solution containing lanthanum and cerium with an atomic ratio of 0.7:0.7 into the transparent ultrafine particle solution for uniform mutual dissolution, stir for 1 hour, and set aside;
[0018] c. Add the manganese-containing solution of the transition metal oxide with an atomic ratio of 1.0 to the solution obtained in step b to dissolve evenly, stir for 1 hour, and set aside;
[0019] d. Evaporate the solution obtained in s...
Embodiment 2
[0021] a. First prepare a kinetically stable titanium dioxide ultrafine particle aqueous solution:
[0022] Slowly add 4 grams of hydrolyzable titanium-containing compound tetraalkoxytitanium into 285ml of deionized water at 15°C, and under the action of ultrasonic waves, the hydrolyzable titanium-containing compound is hydrolyzed and dispersed into a particle size of 10 nanometers -9 For rice-level ultrafine particles, the aqueous solution of ultrafine particles is clarified and transparent under visible light for use;
[0023] b. Add the rare metal solution containing lanthanum and cerium with an atomic ratio of 1.0:1.0 into the transparent ultrafine particle solution for uniform mutual dissolution, stir for 1.5 hours, and set aside;
[0024] c. Add the iron-containing solution of the transition metal oxide with an atomic ratio of 0.9 to the solution obtained in step b to dissolve evenly, stir for 1.5 hours, and set aside;
[0025] d. Evaporate the solution obtained in step...
Embodiment 3
[0027] a. First prepare a kinetically stable titanium dioxide ultrafine particle aqueous solution:
[0028] Slowly add 4.3 grams of hydrolyzable titanium-containing compound titanium tetrachloride into 220ml of deionized water at 10°C. Under the action of ultrasonic waves, the hydrolyzable titanium-containing compound is hydrolyzed and dispersed into a particle size of 10 nanometers. -9 For rice-level ultrafine particles, the aqueous solution of ultrafine particles is clarified and transparent under visible light for use;
[0029] b. Add the rare metal solution containing lanthanum and cerium with an atomic ratio of 1.2:1.2 into the transparent ultrafine particle solution for uniform mutual solubility, stir for 2 hours, and set aside;
[0030] c. Add the cobalt-containing solution of the transition metal oxide with an atomic ratio of 0.7 to the solution obtained in step b to dissolve evenly, stir for 2 hours, and set aside;
[0031] d. Evaporate the solution obtained in step ...
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