Method for detecting impurities in medical PVC sheet processing auxiliary materials
A detection method and a technology for auxiliary materials, applied in the detection field, can solve the problems of unsatisfactory separation of impurities, low separation degree of impurities, and high detection value of vinyl chloride residues, and achieve good economic and social benefits, the method is simple and easy to implement, and the technical support is good. Effect
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[0059] The method for detecting impurities in medical PVC sheet processing auxiliary materials according to the present invention comprises the following steps:
[0060] 1. Preparation of Vinyl Chloride Control Solution
[0061] According to GB / T4615-2013 "Determination of Residual Vinyl Chloride Monomer in Polyvinyl Chloride by Gas Chromatography", the preparation of the vinyl chloride reference solution was carried out.
[0062] Specifically, add 20 mL of DMA (N,N-dimethylaniline) into a 30 mL injection bottle with a pipette, and inject vinyl chloride gas into the DMA solution in the injection bottle with an airtight syringe pre-flushed 5 times to prepare A stock solution was obtained with a concentration of 2740 mg / L.
[0063] Same as above, add 20 mL of DMA to another 30 mL injection bottle with a pipette for use, and use a microsyringe to pipette 500 μL of the stock solution into the above-mentioned injection bottle to prepare a vinyl chloride standard solution with a co...
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